(E)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

Base Information

Chemical Name:(E)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester
CAS No.:1333151-44-2
Molecular Formula:C₁₄H₁₄ClN₃O₂
Molecular Weight:291.737
Hs Code.:

Synonyms:(E)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

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Chemical Property of (E)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

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Technology Process of (E)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

There total 4 articles about (E)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96088-62-9
isopropyl propiolate

: 52853-74-4
3-(3-chlorophenyl)-1,2,4-triazole

: 1333151-42-0
(Z)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

: 1333151-44-2
(E)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

Guidance literature:: With triethylamine; In acetonitrile; at 90 ℃; Inert atmosphere; Cooling;

Reference yield:

: 2548-79-0
3-chlorothiobenzamide

: 1333151-42-0
(Z)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

: 1333151-44-2
(E)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 24 h

2: N,N-dimethyl-formamide / 90 °C / Inert atmosphere

3: triethylamine / acetonitrile / 90 °C / Inert atmosphere; Cooling

With triethylamine; In diethyl ether; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 764621-09-2
C₈H₈ClNS

: 1333151-42-0
(Z)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

: 1333151-44-2
(E)-3-[3-(3-chlorophenyl)-[1,2,4]-triazol-1-yl]acrylic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 90 °C / Inert atmosphere

2: triethylamine / acetonitrile / 90 °C / Inert atmosphere; Cooling

With triethylamine; In N,N-dimethyl-formamide; acetonitrile;