1-((1R,3S)-tetrahydro-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

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Chemical Name:1-((1R,3S)-tetrahydro-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione
CAS No.:287933-88-4
Molecular Formula:C₂₉H₂₈N₂O₅
Molecular Weight:484.552
Hs Code.:

Synonyms:1-((1R,3S)-tetrahydro-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

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Chemical Property of 1-((1R,3S)-tetrahydro-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

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Technology Process of 1-((1R,3S)-tetrahydro-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

There total 4 articles about 1-((1R,3S)-tetrahydro-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 448896-44-4
thiocarbonic acid O-{2-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester O-phenyl ester

: 287933-88-4
1-((1R,3S)-tetrahydro-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 3h; Heating;
DOI:10.1007/s007060200024

Reference yield: 87.0%

: 287934-00-3
1-((1R,2R,3S)-tetrahydro-2-hydroxy-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

: 287933-88-4
1-((1R,3S)-tetrahydro-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

Guidance literature:: 1-((1R,2R,3S)-tetrahydro-2-hydroxy-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione; With O-phenyl chlorothionoformate; In dichloromethane;

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 3h; Heating;
DOI:10.1016/S0040-4039(00)00467-6

Reference yield:

: (S)-4-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-2,6-dioxa-bicyclo[3.1.0]hexane

: 287933-88-4
1-((1R,3S)-tetrahydro-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

Guidance literature:: Multi-step reaction with 3 steps

1: 11 percent / CDCl₃ / 36 h / 20 °C

2: 90 percent / DMAP / CH₂Cl₂ / 3 h / 20 °C

3: 97 percent / AIBN; Bu₃SnH / benzene / 3 h / Heating

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In chloroform-d1; dichloromethane; benzene; 3: Barton-McCombie deoxygenation;
DOI:10.1007/s007060200024