(5aα,6α,9aα,9bα)-9a-Hydroxy-5a-methyl-6-(4-methylphenylsulfonyloxy)-5,5a,6,7,8,9,9a,9b-octahydronaphtho<1,2-b>furan-2(4H)-on

Base Information

Chemical Name:(5aα,6α,9aα,9bα)-9a-Hydroxy-5a-methyl-6-(4-methylphenylsulfonyloxy)-5,5a,6,7,8,9,9a,9b-octahydronaphtho<1,2-b>furan-2(4H)-on
CAS No.:84102-29-4
Molecular Formula:C₂₀H₂₄O₆S
Molecular Weight:392.473
Hs Code.:

Synonyms:(5aα,6α,9aα,9bα)-9a-Hydroxy-5a-methyl-6-(4-methylphenylsulfonyloxy)-5,5a,6,7,8,9,9a,9b-octahydronaphtho<1,2-b>furan-2(4H)-on

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Chemical Property of (5aα,6α,9aα,9bα)-9a-Hydroxy-5a-methyl-6-(4-methylphenylsulfonyloxy)-5,5a,6,7,8,9,9a,9b-octahydronaphtho<1,2-b>furan-2(4H)-on

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Technology Process of (5aα,6α,9aα,9bα)-9a-Hydroxy-5a-methyl-6-(4-methylphenylsulfonyloxy)-5,5a,6,7,8,9,9a,9b-octahydronaphtho<1,2-b>furan-2(4H)-on

There total 10 articles about (5aα,6α,9aα,9bα)-9a-Hydroxy-5a-methyl-6-(4-methylphenylsulfonyloxy)-5,5a,6,7,8,9,9a,9b-octahydronaphtho<1,2-b>furan-2(4H)-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 84102-23-8,84129-94-2
(1aα,2Z,4aβ,5β)-<4a-Methyl-5-(4-methylphenylsulfonyloxy)-4,4a,5,6,7,8-hexahydro-1aH-naphth<1,8a-b>oxiren-2-(3H)-yliden>essigsaeure-methylester

: 84102-29-4
(5aα,6α,9aα,9bα)-9a-Hydroxy-5a-methyl-6-(4-methylphenylsulfonyloxy)-5,5a,6,7,8,9,9a,9b-octahydronaphtho<1,2-b>furan-2(4H)-on

Guidance literature:: With sulfuric acid; In acetone; for 4h; Heating;

Reference yield:

: 32042-78-7
acetic acid (1S*,8aS*)-(+/-)-8a-methyl-6-oxo-1,2,3,4,6,7,8,8a-octahydronaphthalen-1-yl ester

: 84102-29-4
(5aα,6α,9aα,9bα)-9a-Hydroxy-5a-methyl-6-(4-methylphenylsulfonyloxy)-5,5a,6,7,8,9,9a,9b-octahydronaphtho<1,2-b>furan-2(4H)-on

Guidance literature:: Multi-step reaction with 4 steps

1: 30percent H₂O₂, 4N NaOH / methanol / 5 °C

2: 89 percent / pyridine / 72 h / 5 °C

3: 40 percent / NaH / 1,2-dimethoxy-ethane / 6 h / 85 °C

4: 86 percent / 2N H₂SO₄ / acetone / 4 h / Heating

With sodium hydroxide; sulfuric acid; dihydrogen peroxide; sodium hydride; In pyridine; methanol; 1,2-dimethoxyethane; acetone;

Reference yield:

: 50302-16-4
(4aS,5S)-5-Hydroxy-4a-methyl-4,4a,5,6,7,8-hexahydro-3H-naphthalen-2-one

: 84102-29-4
(5aα,6α,9aα,9bα)-9a-Hydroxy-5a-methyl-6-(4-methylphenylsulfonyloxy)-5,5a,6,7,8,9,9a,9b-octahydronaphtho<1,2-b>furan-2(4H)-on

Guidance literature:: Multi-step reaction with 4 steps

1: 30percent H₂O₂, 4N NaOH / methanol / 5 °C

2: 89 percent / pyridine / 72 h / 5 °C

3: 40 percent / NaH / 1,2-dimethoxy-ethane / 6 h / 85 °C

4: 86 percent / 2N H₂SO₄ / acetone / 4 h / Heating

With sodium hydroxide; sulfuric acid; dihydrogen peroxide; sodium hydride; In pyridine; methanol; 1,2-dimethoxyethane; acetone;