3,3'-((6,6'-(ethane-1,2-diylbis(azanediyl))bis(4-(mesityloxy)-1,3,5-triazine-6,2-diyl))bis(azanediyl))dibenzonitrile

Base Information

Chemical Name:3,3'-((6,6'-(ethane-1,2-diylbis(azanediyl))bis(4-(mesityloxy)-1,3,5-triazine-6,2-diyl))bis(azanediyl))dibenzonitrile
CAS No.:1415319-91-3
Molecular Formula:C₄₀H₃₈N₁₂O₂
Molecular Weight:718.821
Hs Code.:

Synonyms:3,3'-((6,6'-(ethane-1,2-diylbis(azanediyl))bis(4-(mesityloxy)-1,3,5-triazine-6,2-diyl))bis(azanediyl))dibenzonitrile

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Chemical Property of 3,3'-((6,6'-(ethane-1,2-diylbis(azanediyl))bis(4-(mesityloxy)-1,3,5-triazine-6,2-diyl))bis(azanediyl))dibenzonitrile

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Technology Process of 3,3'-((6,6'-(ethane-1,2-diylbis(azanediyl))bis(4-(mesityloxy)-1,3,5-triazine-6,2-diyl))bis(azanediyl))dibenzonitrile

There total 3 articles about 3,3'-((6,6'-(ethane-1,2-diylbis(azanediyl))bis(4-(mesityloxy)-1,3,5-triazine-6,2-diyl))bis(azanediyl))dibenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415319-53-7
3-((4-chloro-6-(mesityloxy)-1,3,5-triazin-2-yl)amino)benzonitrile

: 107-15-3,85404-18-8
ethylenediamine

: 1415319-91-3
3,3'-((6,6'-(ethane-1,2-diylbis(azanediyl))bis(4-(mesityloxy)-1,3,5-triazine-6,2-diyl))bis(azanediyl))dibenzonitrile

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 110 ℃; for 48h;
DOI:10.1016/j.bmcl.2012.09.066

Reference yield:

: 1415319-53-7
3-((4-chloro-6-(mesityloxy)-1,3,5-triazin-2-yl)amino)benzonitrile

: 3-(4-(2-aminoethylamino)-6-(mesityloxy)-1,3,5-triazin-2-ylamino)benzonitrile

: 1415319-91-3
3,3'-((6,6'-(ethane-1,2-diylbis(azanediyl))bis(4-(mesityloxy)-1,3,5-triazine-6,2-diyl))bis(azanediyl))dibenzonitrile

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; for 24h; Heating;
DOI:10.1016/j.ejmech.2017.11.075

Reference yield:

: 1415319-53-7
3-((4-chloro-6-(mesityloxy)-1,3,5-triazin-2-yl)amino)benzonitrile

: 1415319-91-3
3,3'-((6,6'-(ethane-1,2-diylbis(azanediyl))bis(4-(mesityloxy)-1,3,5-triazine-6,2-diyl))bis(azanediyl))dibenzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 48 h / 110 °C

2: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 24 h / Heating

With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane;
DOI:10.1016/j.ejmech.2017.11.075