4-(Trifluoromethyl)-N-(4-methylphenyl)-o-phenylenediamine

Base Information

Chemical Name:4-(Trifluoromethyl)-N-(4-methylphenyl)-o-phenylenediamine
CAS No.:637041-68-0
Molecular Formula:C₁₄H₁₃F₃N₂
Molecular Weight:266.266
Hs Code.:
DSSTox Substance ID:DTXSID801193434
Nikkaji Number:J1.937.009G

Synonyms:4-(Trifluoromethyl)-N-(4-methylphenyl)-o-phenylenediamine;XLFPDRYZGDSUDO-UHFFFAOYSA-N;DTXSID801193434;N1-(4-Methylphenyl)-4-(trifluoromethyl)-1,2-benzenediamine;637041-68-0

Suppliers and Price of 4-(Trifluoromethyl)-N-(4-methylphenyl)-o-phenylenediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(Trifluoromethyl)-N-(4-methylphenyl)-o-phenylenediamine

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:266.10308291
Heavy Atom Count:19
Complexity:285

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)NC2=C(C=C(C=C2)C(F)(F)F)N

Technology Process of 4-(Trifluoromethyl)-N-(4-methylphenyl)-o-phenylenediamine

There total 5 articles about 4-(Trifluoromethyl)-N-(4-methylphenyl)-o-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1598-33-0
N-(4-methylphenyl)-2-nitro-4-(trifluoromethyl)aniline

: 637041-68-0
N¹-(4-methylphenyl)-4-(trifluoromethyl)benzene-1,2-diamine

Guidance literature:: With hydrogen; palladium dihydroxide; In methanol; for 24h; under 760 Torr;
DOI:10.1055/s-2003-40888

Reference yield:

: 367-86-2
1-fluoro-2-nitro-4-trifluoromethyl-benzene

: 637041-68-0
N¹-(4-methylphenyl)-4-(trifluoromethyl)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / iPr₂NEt / dimethylsulfoxide / 16 h / 70 °C

2: H₂ / 20 percent Pd(OH)2/C / methanol / 24 h / 760 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium dihydroxide; In methanol; dimethyl sulfoxide;
DOI:10.1055/s-2003-40888

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 637041-68-0
N¹-(4-methylphenyl)-4-(trifluoromethyl)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / iPr₂NEt / dimethylsulfoxide / 16 h / 70 °C

2: H₂ / 20 percent Pd(OH)2/C / methanol / 24 h / 760 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium dihydroxide; In methanol; dimethyl sulfoxide;
DOI:10.1055/s-2003-40888