ethyl (E)-4-[3'-(1-adamantyl)-4'-hydroxyphenyl]-3-(3'-aminopropoxy)cinnamate

Base Information

Chemical Name:ethyl (E)-4-[3'-(1-adamantyl)-4'-hydroxyphenyl]-3-(3'-aminopropoxy)cinnamate
CAS No.:540779-43-9
Molecular Formula:C₃₀H₃₇NO₄
Molecular Weight:475.628
Hs Code.:

Synonyms:ethyl (E)-4-[3'-(1-adamantyl)-4'-hydroxyphenyl]-3-(3'-aminopropoxy)cinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (E)-4-[3'-(1-adamantyl)-4'-hydroxyphenyl]-3-(3'-aminopropoxy)cinnamate

Chemical Property:

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Technology Process of ethyl (E)-4-[3'-(1-adamantyl)-4'-hydroxyphenyl]-3-(3'-aminopropoxy)cinnamate

There total 14 articles about ethyl (E)-4-[3'-(1-adamantyl)-4'-hydroxyphenyl]-3-(3'-aminopropoxy)cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1566621-63-3
C₄₁H₅₉NO₆Si

: 540779-43-9
ethyl (E)-4-[3'-(1-adamantyl)-4'-hydroxyphenyl]-3-(3'-aminopropoxy)cinnamate

Guidance literature:: With hydrogenchloride; In ethanol; at 85 ℃; for 8h; Inert atmosphere;
DOI:10.1016/j.bmc.2014.01.006

Reference yield:

: 540779-38-2
ethyl (E)-4-bromo-3-hydroxycinnamate

: 540779-43-9
ethyl (E)-4-[3'-(1-adamantyl)-4'-hydroxyphenyl]-3-(3'-aminopropoxy)cinnamate

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / K₂CO₃ / acetone / 20 h / Heating

2: 83 percent / Pd(PPh₃)4; aq. Na₂CO₃ / 1,2-dimethoxy-ethane / 20 h / Heating

3: BBr₃ / CH₂Cl₂ / 2 h / -78 °C

4: 278 mg / aq. HCl / ethanol / 2 h / Heating

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; sodium carbonate; potassium carbonate; In 1,2-dimethoxyethane; ethanol; dichloromethane; acetone;
DOI:10.1021/jm030524k