(+/-)methyl 11-(2,4-dichlorophenyl)-3-hydroxy-3-methoxycarbonyl-5-oxo-undecanoate

Base Information

Chemical Name:(+/-)methyl 11-(2,4-dichlorophenyl)-3-hydroxy-3-methoxycarbonyl-5-oxo-undecanoate
CAS No.:180622-68-8
Molecular Formula:C₂₀H₂₆Cl₂O₆
Molecular Weight:433.329
Hs Code.:

Synonyms:(+/-)methyl 11-(2,4-dichlorophenyl)-3-hydroxy-3-methoxycarbonyl-5-oxo-undecanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)methyl 11-(2,4-dichlorophenyl)-3-hydroxy-3-methoxycarbonyl-5-oxo-undecanoate

Chemical Property:

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Technology Process of (+/-)methyl 11-(2,4-dichlorophenyl)-3-hydroxy-3-methoxycarbonyl-5-oxo-undecanoate

There total 3 articles about (+/-)methyl 11-(2,4-dichlorophenyl)-3-hydroxy-3-methoxycarbonyl-5-oxo-undecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 180622-67-7
(+/-)5-(Carbomethoxymethyl)-3-[6-(2, 4-dichlorophenyl)-hexyl]-5-methoxycarbonyl-4,5-dihydroisoxazole

: 180622-68-8
(+/-)methyl 11-(2,4-dichlorophenyl)-3-hydroxy-3-methoxycarbonyl-5-oxo-undecanoate

Guidance literature:: With hydrogen; boric acid; nickel; In methanol; water; for 2h; under 2585.7 Torr; Ambient temperature;
DOI:10.1021/jm960167w

Reference yield:

: 617-52-7
Dimethyl itakonate

: 180622-68-8
(+/-)methyl 11-(2,4-dichlorophenyl)-3-hydroxy-3-methoxycarbonyl-5-oxo-undecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / aq. NaOCl, Et₃N / CH₂Cl₂ / 40 h / Ambient temperature

2: 85 percent / H₂, H₃BO₃ / Raney-Ni / methanol; H₂O / 2 h / 2585.7 Torr / Ambient temperature

With sodium hypochlorite; hydrogen; boric acid; triethylamine; nickel; In methanol; dichloromethane; water;
DOI:10.1021/jm960167w

Reference yield:

: 7-(2,4-Dichloro-phenyl)-heptanal oxime

: 180622-68-8
(+/-)methyl 11-(2,4-dichlorophenyl)-3-hydroxy-3-methoxycarbonyl-5-oxo-undecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / aq. NaOCl, Et₃N / CH₂Cl₂ / 40 h / Ambient temperature

2: 85 percent / H₂, H₃BO₃ / Raney-Ni / methanol; H₂O / 2 h / 2585.7 Torr / Ambient temperature

With sodium hypochlorite; hydrogen; boric acid; triethylamine; nickel; In methanol; dichloromethane; water;
DOI:10.1021/jm960167w