2-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-4,5,6,7-tetrafluorobenzothiazole

Base Information

Chemical Name:2-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-4,5,6,7-tetrafluorobenzothiazole
CAS No.:1418196-18-5
Molecular Formula:C₁₃HF₈NOS
Molecular Weight:371.21
Hs Code.:

Synonyms:2-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-4,5,6,7-tetrafluorobenzothiazole

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Chemical Property of 2-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-4,5,6,7-tetrafluorobenzothiazole

Chemical Property:

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Technology Process of 2-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-4,5,6,7-tetrafluorobenzothiazole

There total 3 articles about 2-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-4,5,6,7-tetrafluorobenzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1418196-16-3
2-(3,4,5,6-tetrafluoro-2-methoxyphenyl)-4,5,6,7-tetrafluorobenzothiazole

: 1418196-18-5
2-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-4,5,6,7-tetrafluorobenzothiazole

Guidance literature:: With boron tribromide; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ic302063u

Reference yield:

: 358352-95-1
2-Methoxy-3,4,5,6-tetrafluorobenzoyl chloride

: 1418196-18-5
2-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-4,5,6,7-tetrafluorobenzothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 24 h / 20 °C / Inert atmosphere

2: tetraphosphorus decasulfide / 1,4-dioxane / 20 h / Inert atmosphere; Reflux

3: boron tribromide / dichloromethane / 2 h / 20 °C

With tetraphosphorus decasulfide; boron tribromide; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ic302063u

Reference yield:

: 771-60-8
2,3,4,5,6-pentafluoroaniline

: 1418196-18-5
2-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-4,5,6,7-tetrafluorobenzothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 24 h / 20 °C / Inert atmosphere

2: tetraphosphorus decasulfide / 1,4-dioxane / 20 h / Inert atmosphere; Reflux

3: boron tribromide / dichloromethane / 2 h / 20 °C

With tetraphosphorus decasulfide; boron tribromide; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ic302063u