octa(p-(tert-butyl)phenyl) cobalt(III) corrolazine

Base Information

Chemical Name:octa(p-(tert-butyl)phenyl) cobalt(III) corrolazine
CAS No.:457883-60-2
Molecular Formula:C₉₆H₁₀₄CoN₇
Molecular Weight:1414.92
Hs Code.:

Synonyms:octa(p-(tert-butyl)phenyl) cobalt(III) corrolazine

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Chemical Property of octa(p-(tert-butyl)phenyl) cobalt(III) corrolazine

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Technology Process of octa(p-(tert-butyl)phenyl) cobalt(III) corrolazine

There total 1 articles about octa(p-(tert-butyl)phenyl) cobalt(III) corrolazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 370569-23-6
octakis(para-tert-butylphenyl)corrolazine

: cobalt(II) aceylacetonate

: 457883-60-2
octa(p-(tert-butyl)phenyl) cobalt(III) corrolazine

Guidance literature:: In pyridine; Co(acac)2 in pyridine was heated with ligand at 115°C for 1 h; pyridine was removed under vac., column chromy. on silica gel with hexane/CH2Cl2;
DOI:10.1021/ic020297x

Reference yield: 83.0%

: 457883-60-2
octa(p-(tert-butyl)phenyl) cobalt(III) corrolazine

: 603-35-0
triphenylphosphine

: 457883-61-3
Co(C₄H₉C₆H₄)8C₁₆N₇(P(C₆H₅)3)

Guidance literature:: In pyridine; PPh3 was added in Co-complex in pyridine, refluxed at 115°C for 1h; pyridine was removed under vac., column chromy. on silica gel with hexane/CH2Cl2;
DOI:10.1021/ic020297x

Reference yield: 71.0%

: 110-86-1
pyridine

: 773837-37-9
sodium cyanide

: 457883-60-2
octa(p-(tert-butyl)phenyl) cobalt(III) corrolazine

: 7732-18-5
water

: octa(p-(tert-butyl)phenyl) cobalt corrolazine cyanide monohydrate

Guidance literature:: With air; In pyridine; water; an aq. soln. of NaCN added to a stirred soln. of Co complex in pyridine,stirred for 30 min at room temp.; evapd. (vac.), dissolved in CH2Cl2, chromd. (silica gel, CH2Cl2); elem. anal.;
DOI:10.1021/ja036983s