2-[5-(3,5-dimethylbenzylcarbamoyl)thiophen-2-yl]-2-oxoethyl ethyl trithiocarbonate

Base Information

Chemical Name:2-[5-(3,5-dimethylbenzylcarbamoyl)thiophen-2-yl]-2-oxoethyl ethyl trithiocarbonate
CAS No.:1039454-47-1
Molecular Formula:C₁₉H₂₁NO₂S₄
Molecular Weight:423.645
Hs Code.:

Synonyms:2-[5-(3,5-dimethylbenzylcarbamoyl)thiophen-2-yl]-2-oxoethyl ethyl trithiocarbonate

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Chemical Property of 2-[5-(3,5-dimethylbenzylcarbamoyl)thiophen-2-yl]-2-oxoethyl ethyl trithiocarbonate

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Technology Process of 2-[5-(3,5-dimethylbenzylcarbamoyl)thiophen-2-yl]-2-oxoethyl ethyl trithiocarbonate

There total 1 articles about 2-[5-(3,5-dimethylbenzylcarbamoyl)thiophen-2-yl]-2-oxoethyl ethyl trithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 4066-41-5
5-acetylthiophene-2-carboxylic acid

: 78710-55-1
3,5-dimethylbenzyl amine

: 67715-76-8
sodium ethyltrithiocarbonate

: 1039454-47-1
2-[5-(3,5-dimethylbenzylcarbamoyl)thiophen-2-yl]-2-oxoethyl ethyl trithiocarbonate

Guidance literature:: 5-acetylthiophene-2-carboxylic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at 0 ℃; for 0.75h;

3,5-dimethylbenzyl amine; In tetrahydrofuran; at 20 ℃; for 18h;

sodium ethyltrithiocarbonate; Further stages;
DOI:10.1021/jm800093c