3-(2-{2-[2-(tert-butyldimethylsilanyloxy)ethoxy]ethoxy}ethoxy)-4-methoxybenzaldehyde

Base Information

Chemical Name:3-(2-{2-[2-(tert-butyldimethylsilanyloxy)ethoxy]ethoxy}ethoxy)-4-methoxybenzaldehyde
CAS No.:886449-59-8
Molecular Formula:C₂₀H₃₄O₆Si
Molecular Weight:398.572
Hs Code.:

Synonyms:3-(2-{2-[2-(tert-butyldimethylsilanyloxy)ethoxy]ethoxy}ethoxy)-4-methoxybenzaldehyde

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Chemical Property of 3-(2-{2-[2-(tert-butyldimethylsilanyloxy)ethoxy]ethoxy}ethoxy)-4-methoxybenzaldehyde

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Technology Process of 3-(2-{2-[2-(tert-butyldimethylsilanyloxy)ethoxy]ethoxy}ethoxy)-4-methoxybenzaldehyde

There total 3 articles about 3-(2-{2-[2-(tert-butyldimethylsilanyloxy)ethoxy]ethoxy}ethoxy)-4-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}-4-methoxybenzaldehyde

: 18162-48-6
tert-butyldimethylsilyl chloride

: 886449-59-8
3-(2-{2-[2-(tert-butyldimethylsilanyloxy)ethoxy]ethoxy}ethoxy)-4-methoxybenzaldehyde

Guidance literature:: With 1H-imidazole; In dichloromethane; at 25 ℃; for 5h;
DOI:10.1039/b517933e

Reference yield:

: 621-59-0
isovanillin

: 886449-59-8
3-(2-{2-[2-(tert-butyldimethylsilanyloxy)ethoxy]ethoxy}ethoxy)-4-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / K₂CO₃ / acetone / 12 h / Heating

2: 82 percent / imidazole / CH₂Cl₂ / 5 h / 25 °C

With 1H-imidazole; potassium carbonate; In dichloromethane; acetone;
DOI:10.1039/b517933e

Reference yield:

: 77544-68-4
8-tosyloxy-3,6-dioxaoctanol

: 886449-59-8
3-(2-{2-[2-(tert-butyldimethylsilanyloxy)ethoxy]ethoxy}ethoxy)-4-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / K₂CO₃ / acetone / 12 h / Heating

2: 82 percent / imidazole / CH₂Cl₂ / 5 h / 25 °C

With 1H-imidazole; potassium carbonate; In dichloromethane; acetone;
DOI:10.1039/b517933e