4-[di-2,3-tert-butoxycarbonylguanidino]-4’-[di-(tert-butoxycarbonyl)-2-imino-imidazolidino]diphenylmethane

Base Information

Chemical Name:4-[di-2,3-tert-butoxycarbonylguanidino]-4’-[di-(tert-butoxycarbonyl)-2-imino-imidazolidino]diphenylmethane
CAS No.:1196966-11-6
Molecular Formula:C₃₇H₅₂N₆O₈
Molecular Weight:708.855
Hs Code.:

Synonyms:4-[di-2,3-tert-butoxycarbonylguanidino]-4’-[di-(tert-butoxycarbonyl)-2-imino-imidazolidino]diphenylmethane

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Chemical Property of 4-[di-2,3-tert-butoxycarbonylguanidino]-4’-[di-(tert-butoxycarbonyl)-2-imino-imidazolidino]diphenylmethane

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Technology Process of 4-[di-2,3-tert-butoxycarbonylguanidino]-4’-[di-(tert-butoxycarbonyl)-2-imino-imidazolidino]diphenylmethane

There total 3 articles about 4-[di-2,3-tert-butoxycarbonylguanidino]-4’-[di-(tert-butoxycarbonyl)-2-imino-imidazolidino]diphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1196966-03-6
4-amino-4’-[2,3-di(tert-butoxycarbonyl)guanidino]diphenylmethane

: 173300-83-9
2-thioxo-imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester

: 1196966-11-6
4-[di-2,3-tert-butoxycarbonylguanidino]-4’-[di-(tert-butoxycarbonyl)-2-imino-imidazolidino]diphenylmethane

Guidance literature:: With triethylamine; mercury dichloride; In dichloromethane; at 20 ℃;
DOI:10.1016/j.ejmech.2020.112947

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1196966-11-6
4-[di-2,3-tert-butoxycarbonylguanidino]-4’-[di-(tert-butoxycarbonyl)-2-imino-imidazolidino]diphenylmethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran; mineral oil / 0.25 h / 0 - 20 °C / Inert atmosphere

1.2: 16.5 h / 0 - 20 °C / Inert atmosphere

2.1: triethylamine; mercury dichloride / dichloromethane / 20 °C

With triethylamine; mercury dichloride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1016/j.ejmech.2020.112947

Reference yield:

: 145013-05-4
tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate

: 1196966-11-6
4-[di-2,3-tert-butoxycarbonylguanidino]-4’-[di-(tert-butoxycarbonyl)-2-imino-imidazolidino]diphenylmethane

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; mercury dichloride / dichloromethane / 20 °C

2: triethylamine; mercury dichloride / dichloromethane / 20 °C

With triethylamine; mercury dichloride; In dichloromethane;
DOI:10.1016/j.ejmech.2020.112947