methyl 2-cyano-1-<(2-phenylsulfonyl)vinyl>-2-(trimethylsiloxy)cyclohexanecarboxylate

Base Information

Chemical Name:methyl 2-cyano-1-<(2-phenylsulfonyl)vinyl>-2-(trimethylsiloxy)cyclohexanecarboxylate
CAS No.:83219-98-1
Molecular Formula:C₂₀H₂₇NO₅SSi
Molecular Weight:421.59
Hs Code.:

Synonyms:methyl 2-cyano-1-<(2-phenylsulfonyl)vinyl>-2-(trimethylsiloxy)cyclohexanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-cyano-1-<(2-phenylsulfonyl)vinyl>-2-(trimethylsiloxy)cyclohexanecarboxylate

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Technology Process of methyl 2-cyano-1-<(2-phenylsulfonyl)vinyl>-2-(trimethylsiloxy)cyclohexanecarboxylate

There total 1 articles about methyl 2-cyano-1-<(2-phenylsulfonyl)vinyl>-2-(trimethylsiloxy)cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 7677-24-9
trimethylsilyl cyanide

: 83219-83-4,83219-92-5
methyl 2-oxo-1-<(2-phenylsulfonyl)vinyl>cyclohexanecarboxylate

: 83219-98-1
methyl 2-cyano-1-<(2-phenylsulfonyl)vinyl>-2-(trimethylsiloxy)cyclohexanecarboxylate

Guidance literature:: With zinc(II) iodide; In dichloromethane; for 96h; Ambient temperature;
DOI:10.1021/jo00145a020

Reference yield:

: 83219-98-1
methyl 2-cyano-1-<(2-phenylsulfonyl)vinyl>-2-(trimethylsiloxy)cyclohexanecarboxylate

: 83219-84-5
2-Cyano-2-trimethylsilanyloxy-1-vinyl-cyclohexanecarboxylic acid methyl ester

Guidance literature:: With aluminum amalgam; In tetrahydrofuran; water; at 0 - 20 ℃; for 48h; Yield given;
DOI:10.1021/jo00145a020

Reference yield:

: 83219-98-1
methyl 2-cyano-1-<(2-phenylsulfonyl)vinyl>-2-(trimethylsiloxy)cyclohexanecarboxylate

: 83219-85-6
methyl 2-oxo-1-vinylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Al(Hg) / tetrahydrofuran; H₂O / 48 h / 0 - 20 °C

2: AgF / tetrahydrofuran; H₂O / 5 h / 40 °C

With aluminum amalgam; silver fluoride; In tetrahydrofuran; water;
DOI:10.1021/jo00145a020