4-(boronic acid pinacolate ester)-4-phenyl-2-butene

Base Information

Chemical Name:4-(boronic acid pinacolate ester)-4-phenyl-2-butene
CAS No.:1356467-99-6
Molecular Formula:C₁₆H₂₃BO₂
Molecular Weight:258.168
Hs Code.:

Synonyms:4-(boronic acid pinacolate ester)-4-phenyl-2-butene

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Chemical Property of 4-(boronic acid pinacolate ester)-4-phenyl-2-butene

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Technology Process of 4-(boronic acid pinacolate ester)-4-phenyl-2-butene

There total 6 articles about 4-(boronic acid pinacolate ester)-4-phenyl-2-butene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4,4,5,5-tetramethyl-2-(1-phenylbut-3-en-1-yl)-1,3,2-dioxaborolane

: 1356467-99-6
4-(boronic acid pinacolate ester)-4-phenyl-2-butene

: 4,4,5,5-tetramethyl-2-(1-phenylbut-1-enyl)-[1,3,2]dioxaborolane

Guidance literature:: With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); In tetrahydrofuran; at 60 ℃; for 16h; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/d0sc02542a

Reference yield:

: 157339-09-8
carbonic acid methyl ester 1-phenyl-but-3-enyl ester

: 73183-34-3
bis(pinacol)diborane

: (2E)-2-(4-phenylbut-3-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1356467-99-6
4-(boronic acid pinacolate ester)-4-phenyl-2-butene

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; P(p-CH₃OC₆H₄)3; In N,N-dimethyl acetamide; acetonitrile; at 60 ℃; for 48h; Reagent/catalyst; Solvent; Overall yield = 65 percent; Overall yield = 83.2 mg; regioselective reaction; Catalytic behavior;
DOI:10.1246/cl.210051

Reference yield:

: 1515-78-2
buta-1,3-dien-1-ylbenzene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1356467-99-6
4-(boronic acid pinacolate ester)-4-phenyl-2-butene

: C₁₆H₂₃BO₂

Guidance literature:: With sodium triethylborohydride; (S)-4-isopropyl-2-(6-methylpyridin-2-yl)-4,5-dihydrooxazole; cobalt(II) chloride; In tetrahydrofuran; at 25 ℃; for 5h; regioselective reaction;
DOI:10.1007/s11426-018-9418-7