Technology Process of p-<(E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-propenyl>-benzyl acetate
There total 5 articles about p-<(E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-propenyl>-benzyl acetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
diethyl ether;
for 3h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium borohydride / methanol / 1.5 h / 0 °C
2: phosphorus tribromide / pyridine / diethyl ether; hexane / 2.5 h / 0 - 5 °C
3: diethyl ether; xylene / 48 h / 100 °C
4: 69.3 percent / butylene oxide / 12 h / 65 °C
5: 89 percent / lithium aluminum hydride / tetrahydrofuran; diethyl ether / 0 - 5 °C
6: 91 percent / pyridine / diethyl ether / 3 h
With
tetrahydrofuran; pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; phosphorus tribromide;
pyridine;
In
tetrahydrofuran; methanol; diethyl ether; hexane; xylene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: phosphorus tribromide / pyridine / diethyl ether; hexane / 2.5 h / 0 - 5 °C
2: diethyl ether; xylene / 48 h / 100 °C
3: 69.3 percent / butylene oxide / 12 h / 65 °C
4: 89 percent / lithium aluminum hydride / tetrahydrofuran; diethyl ether / 0 - 5 °C
5: 91 percent / pyridine / diethyl ether / 3 h
With
tetrahydrofuran; pyridine; lithium aluminium tetrahydride; phosphorus tribromide;
pyridine;
In
tetrahydrofuran; diethyl ether; hexane; xylene;
