4-acetyl-1,5-dibenzyloxy-3-hydroxy-2-C-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)benzene

Base Information

Chemical Name:4-acetyl-1,5-dibenzyloxy-3-hydroxy-2-C-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)benzene
CAS No.:250273-70-2
Molecular Formula:C₅₆H₅₄O₉
Molecular Weight:871.039
Hs Code.:

Synonyms:4-acetyl-1,5-dibenzyloxy-3-hydroxy-2-C-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)benzene

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Chemical Property of 4-acetyl-1,5-dibenzyloxy-3-hydroxy-2-C-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)benzene

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Technology Process of 4-acetyl-1,5-dibenzyloxy-3-hydroxy-2-C-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)benzene

There total 2 articles about 4-acetyl-1,5-dibenzyloxy-3-hydroxy-2-C-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 18065-05-9
1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone

: 78153-79-4,89025-46-7,94898-43-8,101966-50-1,122741-44-0,143615-35-4,94898-42-7
2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl fluoride

: 250273-70-2
4-acetyl-1,5-dibenzyloxy-3-hydroxy-2-C-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)benzene

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; at -78 - 20 ℃; for 1.75h;
DOI:10.1016/S0008-6215(99)00140-8

Reference yield: 13.0%

: 18065-05-9
1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone

: 78153-79-4,89025-46-7,94898-43-8,101966-50-1,122741-44-0,143615-35-4,94898-42-7
2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl fluoride

: 250273-70-2
4-acetyl-1,5-dibenzyloxy-3-hydroxy-2-C-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)benzene

: 4,6-bis-benzyloxy-2-hydroxy-3-C-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)acetophenone

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -78 - 0 ℃; for 2.5h;
DOI:10.1016/S0008-6215(01)00076-3

Reference yield: 100.0%

: 250273-70-2
4-acetyl-1,5-dibenzyloxy-3-hydroxy-2-C-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl)benzene

: 4-acetyl-1,3,5-trihydroxy-2-C-(β-D-mannopyranosyl)benzene

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; at 20 ℃; for 24h;
DOI:10.1016/S0008-6215(99)00140-8