erythro-3-(p-hydroxyphenyl)-4-hexestrol

Base Information

Chemical Name:erythro-3-(p-hydroxyphenyl)-4-hexestrol
CAS No.:76412-11-8
Molecular Formula:C₁₉H₂₃ClO
Molecular Weight:302.844
Hs Code.:

erythro-3-(p-hydroxyphenyl)-4-<p-(chloromethyl)phenyl>hexestrol

Synonyms:erythro-3-(p-hydroxyphenyl)-4-hexestrol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of erythro-3-(p-hydroxyphenyl)-4-hexestrol

Chemical Property:

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Technology Process of erythro-3-(p-hydroxyphenyl)-4-hexestrol

There total 7 articles about erythro-3-(p-hydroxyphenyl)-4-hexestrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 39952-71-1
erythro-3-(p-hydroxyphenyl)-4-hexane

: 76412-11-8
erythro-3-(p-hydroxyphenyl)-4-hexestrol

Guidance literature:: With hydrogenchloride; In ethanol; Heating;
DOI:10.1021/jm00136a013

Reference yield:

: 84-16-2,26614-21-1
hexestrol

: 76412-11-8
erythro-3-(p-hydroxyphenyl)-4-hexestrol

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) K₂CO₃, 2.) H₂ / 2.) 5percent Pd/C / 1.) acetone, reflux, 17 h, 2.) ethanol, 37 psi, 35 deg C

2: 90 percent / pyridine / Ambient temperature

3: 59 percent / AlCl₃ / CH₂Cl₂ / 3 h / 0 °C

4: 87 percent / LiAlH₄ / tetrahydrofuran / 0 °C

5: 96 percent / HCl gas / ethanol / Heating

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm00136a013

Reference yield:

: 3929-22-4,5776-73-8,5776-74-9
deoxyhexestrol

: 76412-11-8
erythro-3-(p-hydroxyphenyl)-4-hexestrol

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / pyridine / Ambient temperature

2: 59 percent / AlCl₃ / CH₂Cl₂ / 3 h / 0 °C

3: 87 percent / LiAlH₄ / tetrahydrofuran / 0 °C

4: 96 percent / HCl gas / ethanol / Heating

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm00136a013