(E)-1-<2-<(5-benzyloxy)-4-(1-methylethyl)-2-nitrophenyl>ethenyl>pyrrolidine

Base Information

Chemical Name:(E)-1-<2-<(5-benzyloxy)-4-(1-methylethyl)-2-nitrophenyl>ethenyl>pyrrolidine
CAS No.:159388-66-6
Molecular Formula:C₂₂H₂₆N₂O₃
Molecular Weight:366.46
Hs Code.:

Synonyms:(E)-1-<2-<(5-benzyloxy)-4-(1-methylethyl)-2-nitrophenyl>ethenyl>pyrrolidine

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Chemical Property of (E)-1-<2-<(5-benzyloxy)-4-(1-methylethyl)-2-nitrophenyl>ethenyl>pyrrolidine

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Technology Process of (E)-1-<2-<(5-benzyloxy)-4-(1-methylethyl)-2-nitrophenyl>ethenyl>pyrrolidine

There total 3 articles about (E)-1-<2-<(5-benzyloxy)-4-(1-methylethyl)-2-nitrophenyl>ethenyl>pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 123-75-1
pyrrolidine

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 159388-65-5
4-benzyloxy-2-methyl-5-(1-methylethyl)nitrobenzene

: 159388-66-6
(E)-1-<2-<(5-benzyloxy)-4-(1-methylethyl)-2-nitrophenyl>ethenyl>pyrrolidine

Guidance literature:: In N,N-dimethyl-formamide; at 110 ℃; for 4h;
DOI:10.1016/0223-5234(94)90147-3

Reference yield:

: 36778-56-0
5-methyl-2-(1-methylethyl)4-nitrophenol

: 159388-66-6
(E)-1-<2-<(5-benzyloxy)-4-(1-methylethyl)-2-nitrophenyl>ethenyl>pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / K₂CO₃ / dimethylformamide / 3.5 h / 90 °C

2: 90 percent / dimethylformamide / 4 h / 110 °C

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(94)90147-3

Reference yield:

: 100-44-7
benzyl chloride

: 159388-66-6
(E)-1-<2-<(5-benzyloxy)-4-(1-methylethyl)-2-nitrophenyl>ethenyl>pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / K₂CO₃ / dimethylformamide / 3.5 h / 90 °C

2: 90 percent / dimethylformamide / 4 h / 110 °C

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(94)90147-3