C₃₀H₂₉ClFN₃O₆

Base Information

Chemical Name:C₃₀H₂₉ClFN₃O₆
CAS No.:1622396-75-1
Molecular Formula:C₃₀H₂₉ClFN₃O₆
Molecular Weight:582.028
Hs Code.:

C<sub>30</sub>H<sub>29</sub>ClFN<sub>3</sub>O<sub>6</sub>

Synonyms:C₃₀H₂₉ClFN₃O₆

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Chemical Property of C₃₀H₂₉ClFN₃O₆

Chemical Property:

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Technology Process of C₃₀H₂₉ClFN₃O₆

There total 9 articles about C₃₀H₂₉ClFN₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2969-81-5
Ethyl 4-bromobutyrate

: 1622342-89-5
C₃₁H₂₅ClFN₃O₄

: 1622396-75-1
C₃₀H₂₉ClFN₃O₆

: 1622396-76-2
C₃₀H₃₀FN₃O₆

Guidance literature:: C₃₁H₂₅ClFN₃O₄; With hydrogen; palladium(II) hydroxide; In tetrahydrofuran; methanol; for 1.5h; under 2585.81 Torr;

Ethyl 4-bromobutyrate; With potassium carbonate; In N,N-dimethyl-formamide; at 45 ℃; Overall yield = 73 %; Overall yield = 587 mg;

Reference yield:

: 75665-88-2
1-(4-(benzyloxy)-5-methoxy-2-nitrophenyl)ethanone

: 1622396-75-1
C₃₀H₂₉ClFN₃O₆

: 1622396-76-2
C₃₀H₃₀FN₃O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: iron; ammonium acetate / toluene; water / 105 °C

2.1: sodium methylate / 1,2-dimethoxyethane / 0.5 h / Inert atmosphere

2.2: Inert atmosphere

3.1: trichlorophosphate / 10 h / Reflux

4.1: potassium carbonate; sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 100 °C / Inert atmosphere

5.1: triethylamine / dichloromethane; toluene / 1.5 h / -78 - 20 °C

6.1: hydrogen; palladium(II) hydroxide / methanol; tetrahydrofuran / 1.5 h / 2585.81 Torr

6.2: 45 °C

With ammonium acetate; hydrogen; sodium methylate; palladium(II) hydroxide; iron; sodium hydride; potassium carbonate; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 205448-31-3
4-chloro-6-methoxy-7-hydroxyquinoline

: 1622396-75-1
C₃₀H₂₉ClFN₃O₆

: 1622396-76-2
C₃₀H₃₀FN₃O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 45 °C

2.1: potassium carbonate; sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 100 °C / Inert atmosphere

3.1: triethylamine / dichloromethane; toluene / 1.5 h / -78 - 20 °C

4.1: hydrogen; palladium(II) hydroxide / methanol; tetrahydrofuran / 1.5 h / 2585.81 Torr

4.2: 45 °C

With hydrogen; palladium(II) hydroxide; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;