methyl 2,3,4-tri-O-benzyl-6-deoxy-6-[(N'-2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)ureido]-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-6-deoxy-6-[(N'-2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)ureido]-α-D-glucopyranoside
CAS No.:1063748-64-0
Molecular Formula:C₆₃H₆₈N₂O₁₁
Molecular Weight:1029.24
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-6-deoxy-6-[(N'-2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)ureido]-α-D-glucopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzyl-6-deoxy-6-[(N'-2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)ureido]-α-D-glucopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-6-deoxy-6-[(N'-2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)ureido]-α-D-glucopyranoside

There total 4 articles about methyl 2,3,4-tri-O-benzyl-6-deoxy-6-[(N'-2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)ureido]-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 72471-11-5
methyl 6-deoxy-6-amino-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 936132-16-0
1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)formic acid

: 1063748-64-0
methyl 2,3,4-tri-O-benzyl-6-deoxy-6-[(N'-2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)ureido]-α-D-glucopyranoside

Guidance literature:: 1-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)formic acid; With diphenylphosphoranyl azide; triethylamine; In benzene; for 1h; Heating;

methyl 6-deoxy-6-amino-2,3,4-tri-O-benzyl-α-D-glucopyranoside; In acetonitrile; benzene; for 5h; Further stages.; Heating;
DOI:10.1016/j.tet.2008.06.089

Reference yield: 66.0%

: 72471-11-5
methyl 6-deoxy-6-amino-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 99701-64-1
N-((2S,3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)-methyl)-tetrahydro-2H-pyran-2-yl)-2,2,2-trichloroacetamide

: 1063748-64-0
methyl 2,3,4-tri-O-benzyl-6-deoxy-6-[(N'-2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)ureido]-α-D-glucopyranoside

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 25 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.201402433

Reference yield:

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 1063748-64-0
methyl 2,3,4-tri-O-benzyl-6-deoxy-6-[(N'-2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)ureido]-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; silver trifluoromethanesulfonate / dichloromethane / 1 h / 25 °C / Schlenk technique; Inert atmosphere

2: caesium carbonate / N,N-dimethyl-formamide / 25 °C / Schlenk technique; Inert atmosphere

With 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; silver trifluoromethanesulfonate; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201402433