1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol

Base Information

Chemical Name:1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol
CAS No.:1108205-31-7
Molecular Formula:C₂₀H₃₄O₃Si
Molecular Weight:350.574
Hs Code.:

Synonyms:1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol

Suppliers and Price of 1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol

Chemical Property:

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Technology Process of 1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol

There total 1 articles about 1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1108205-27-1
1-[(1S)-1-(tert-butyldimethylsilyloxy)-3-hydroxy-1-methylpropyl]cyclopropanol

: 100-39-0
benzyl bromide

: 1108205-31-7
1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; at 0 - 50 ℃;
DOI:10.1055/s-0028-1083536

Reference yield: 89.0%

: 1108205-31-7
1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol

: 1108205-24-8
(2R)-2-(2-benzyloxyethyl)-2-methylcyclobutanone

Guidance literature:: With 2,6-dimethylpyridine; t-butyldimethylsiyl triflate; In dichloromethane; at -78 ℃; optical yield given as %ee;
DOI:10.1055/s-0028-1083536

Reference yield:

: 1108205-31-7
1-[(1S)-3-(benzyloxy)-1-(tert-butyldimethylsilyloxy)-1-methylpropyl]cyclopropanol

: (2S)-2-(2-benzyloxyethyl)-2-methylcyclobutanone

: 1108205-24-8
(2R)-2-(2-benzyloxyethyl)-2-methylcyclobutanone

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -40 ℃; Reagent/catalyst; Solvent; Temperature; optical yield given as %ee; Reactivity;
DOI:10.1055/s-0028-1083536