1',4'-diphenylspiro

Base Information

• Chemical Name: 1',4'-diphenylspiro
• CAS No.: 73079-03-5
• Molecular Formula: C₂₇H₁₉N₃O
• Molecular Weight: 401.467

Synonyms:1',4'-diphenylspiro

Chemical Property of 1',4'-diphenylspiro

Chemical Property:

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Technology Process of 1',4'-diphenylspiro

There total 1 articles about 1',4'-diphenylspiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

benzylideneanthrone (14343-92-1) + Phenyl azide (622-37-7) → 1',4'-diphenylspiro (73079-03-5)

Guidance literature:

at 90 ℃;

DOI:10.1021/jo01297a028

Reference yield: 40.0%

1',4'-diphenylspiro (73079-03-5) → 9,10-phenanthrenequinone (84-65-1) + 10,11-dihydro-10-phenyl-11-(phenylimino)-5H-dibenzocyclohepten-5-one (73078-92-9) + 10-anilino-11-phenyl-5H-dibenzocyclohepten-5-one (73078-87-2)

Guidance literature:

In benzene; for 3h; Ambient temperature; Irradiation;

DOI:10.1021/jo01297a028

Reference yield: 8.0%

1',4'-diphenylspiro (73079-03-5) → 10,11-dihydro-10-phenyl-11-(phenylimino)-5H-dibenzocyclohepten-5-one (73078-92-9)

Guidance literature:

In xylene; Heating;

DOI:10.1021/jo01297a028

upstream raw materials:

benzylideneanthrone

Phenyl azide

Downstream raw materials:

9,10-phenanthrenequinone

10,11-dihydro-10-phenyl-11-(phenylimino)-5H-dibenzocyclohepten-5-one

10-anilino-11-phenyl-5H-dibenzocyclohepten-5-one

10,11-dihydro-11-phenyl-5H-dibenzocycloheptene-5,10-dione

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