8-<4-<(carboxymethyl)oxy>phenyl>-1,3-diethylxanthine 2-(D-lysylamino)ethylamide dihydrobromide

Base Information

Chemical Name:8-<4-<(carboxymethyl)oxy>phenyl>-1,3-diethylxanthine 2-(D-lysylamino)ethylamide dihydrobromide
CAS No.:104576-56-9
Molecular Formula:2BrH*C₂₅H₃₆N₈O₅
Molecular Weight:690.435
Hs Code.:

Synonyms:8-<4-<(carboxymethyl)oxy>phenyl>-1,3-diethylxanthine 2-(D-lysylamino)ethylamide dihydrobromide

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Chemical Property of 8-<4-<(carboxymethyl)oxy>phenyl>-1,3-diethylxanthine 2-(D-lysylamino)ethylamide dihydrobromide

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Technology Process of 8-<4-<(carboxymethyl)oxy>phenyl>-1,3-diethylxanthine 2-(D-lysylamino)ethylamide dihydrobromide

There total 5 articles about 8-<4-<(carboxymethyl)oxy>phenyl>-1,3-diethylxanthine 2-(D-lysylamino)ethylamide dihydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 104576-55-8
[(R)-5-tert-Butoxycarbonylamino-5-(2-{2-[4-(1,3-diethyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethylcarbamoyl)-pentyl]-carbamic acid benzyl ester

: 104576-56-9
8-<4-<(carboxymethyl)oxy>phenyl>-1,3-diethylxanthine 2-(D-lysylamino)ethylamide dihydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid;
DOI:10.1021/jm00384a037

Reference yield:

: 104576-44-5
[4-(1,3-Diethyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid

: 104576-56-9
8-<4-<(carboxymethyl)oxy>phenyl>-1,3-diethylxanthine 2-(D-lysylamino)ethylamide dihydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / HCl / 50 °C

2: 92 percent / Ambient temperature

3: 79 percent / DCC, HOBt / dimethylformamide

4: 100 percent / 30percent HBr / acetic acid

With hydrogenchloride; hydrogen bromide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00384a037

Reference yield:

: 55878-47-2
(R)-6-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-hexanoic acid

: 104576-56-9
8-<4-<(carboxymethyl)oxy>phenyl>-1,3-diethylxanthine 2-(D-lysylamino)ethylamide dihydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / DCC, HOBt / dimethylformamide

2: 100 percent / 30percent HBr / acetic acid

With hydrogen bromide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00384a037