C₁₈H₁₈O₆

Base Information

Chemical Name:C₁₈H₁₈O₆
CAS No.:1163750-82-0
Molecular Formula:C₁₈H₁₈O₆
Molecular Weight:330.337
Hs Code.:

C<sub>18</sub>H<sub>18</sub>O<sub>6</sub>

Synonyms:C₁₈H₁₈O₆

Suppliers and Price of C₁₈H₁₈O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₈O₆

Chemical Property:

Purity/Quality:

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Technology Process of C₁₈H₁₈O₆

There total 13 articles about C₁₈H₁₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1163751-08-3
C₁₈H₁₈O₅

: 1163750-82-0
C₁₈H₁₈O₆

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; water; In tert-butyl alcohol; at 25 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/anie.200900264

Reference yield:

: 533-31-3
Sesamol

: 1163750-82-0
C₁₈H₁₈O₆

Guidance literature:: Multi-step reaction with 12 steps

1: Inert atmosphere

2: n-butyllithium / Inert atmosphere

3: hydrogenchloride / ethanol; water / Inert atmosphere

4: acetic acid / Inert atmosphere

5: potassium carbonate / Inert atmosphere

6: potassium tert-butylate / Inert atmosphere

7: AD-mix-β; water / Inert atmosphere

8: triethylamine / Inert atmosphere

9: sodium hydride / Inert atmosphere

10: triethylsilane; dichloro-acetic acid / Inert atmosphere

11: oxalyl dichloride; dimethyl sulfoxide / Inert atmosphere

12: sodium dihydrogenphosphate; sodium chlorite / Inert atmosphere

With hydrogenchloride; triethylsilane; dichloro-acetic acid; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; oxalyl dichloride; AD-mix-β; potassium tert-butylate; water; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; triethylamine; In ethanol; water; 4: Duff reaction / 7: Sharpless dihydroxylation / 11: Swern oxidation / 12: Lindgren-Kraus oxidation;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 111726-43-3
3,4-(methylenedioxy)phenyl methoxymethyl ether

: 1163750-82-0
C₁₈H₁₈O₆

Guidance literature:: Multi-step reaction with 11 steps

1: n-butyllithium / Inert atmosphere

2: hydrogenchloride / ethanol; water / Inert atmosphere

3: acetic acid / Inert atmosphere

4: potassium carbonate / Inert atmosphere

5: potassium tert-butylate / Inert atmosphere

6: AD-mix-β; water / Inert atmosphere

7: triethylamine / Inert atmosphere

8: sodium hydride / Inert atmosphere

9: triethylsilane; dichloro-acetic acid / Inert atmosphere

10: oxalyl dichloride; dimethyl sulfoxide / Inert atmosphere

11: sodium dihydrogenphosphate; sodium chlorite / Inert atmosphere

With hydrogenchloride; triethylsilane; dichloro-acetic acid; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; oxalyl dichloride; AD-mix-β; potassium tert-butylate; water; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; triethylamine; In ethanol; water; 3: Duff reaction / 6: Sharpless dihydroxylation / 10: Swern oxidation / 11: Lindgren-Kraus oxidation;
DOI:10.1016/j.tet.2011.04.094