3-(Trimethylsilyl)pent-4-enoic acid

Base Information

Chemical Name:3-(Trimethylsilyl)pent-4-enoic acid
CAS No.:103681-20-5
Molecular Formula:C₈H₁₆O₂Si
Molecular Weight:172.299
Hs Code.:
DSSTox Substance ID:DTXSID40542939
Mol file:103681-20-5.mol

Synonyms:3-(Trimethylsilyl)pent-4-enoic acid;103681-20-5;3-trimethylsilylpent-4-enoic acid;3-Trimethylsilyl-4-pentenoicacid;DTXSID40542939;AKOS006276655

Suppliers and Price of 3-(Trimethylsilyl)pent-4-enoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-TRIMETHYLSILYL-4-PENTENOIC ACID 95.00%
5MG
$ 495.46

Total 3 raw suppliers

Chemical Property of 3-(Trimethylsilyl)pent-4-enoic acid

Chemical Property:

PSA：37.30000
LogP:2.35550
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:172.091956283
Heavy Atom Count:11
Complexity:158

Purity/Quality:

98%Min ^*data from raw suppliers

3-TRIMETHYLSILYL-4-PENTENOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C(CC(=O)O)C=C

Technology Process of 3-(Trimethylsilyl)pent-4-enoic acid

There total 4 articles about 3-(Trimethylsilyl)pent-4-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 86422-21-1
(E)-3-(trimethylsilyl)-2-propenyl acetate

: 103681-20-5
3-Trimethylsilanyl-pent-4-enoic acid

Guidance literature:: DOI:10.1016/S0040-4039(00)98900-7

Reference yield:

: 59376-64-6
(2E)-3-(trimethylsilyl)prop-2-en-1-ol

: 103681-20-5
3-Trimethylsilanyl-pent-4-enoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / Pyridine / tetrahydrofuran / 0 °C

2: 1.) Zn / THF, HMPA

3: 2.) H₂O, H⁽¹⁺⁾ / 2.) heating

With pyridine; water; hydrogen cation; zinc; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)98900-7