3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol

Base Information

Chemical Name:3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol
CAS No.:1124281-27-1
Molecular Formula:C₂₂H₃₄N₂O
Molecular Weight:342.525
Hs Code.:

Synonyms:3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol

Chemical Property:

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Technology Process of 3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol

There total 1 articles about 3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103127-55-5
(S)-(2-cyclohexyl-1-formylethyl)carbamic acid,1,1-dimethylethyl ester

: 949902-73-2
3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-phenol hydrobromide

: 1124281-27-1
3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol

Guidance literature:: (S)-(2-cyclohexyl-1-formylethyl)carbamic acid,1,1-dimethylethyl ester; 3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-phenol hydrobromide; With sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 12h;

With trifluoroacetic acid; In dichloromethane; for 3h;

Reference yield:

: 1124281-27-1
3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol

: 51163-24-7
cyclohexanemethyl isocyanate

: 1124281-58-8
1-cyclohexylmethyl-3-{1-cyclohexylmethyl-2-[3-endo-(3-hydroxyphenyl)-8-azabicyclo[3.2.1]oct-8-yl]ethyl}urea trifluoroacetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 50 ℃;

Reference yield:

: 1124281-27-1
3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol

: 13831-31-7
Acetoxyacetyl chloride

: 1124281-53-3
N-{1-cyclohexylmethyl-2-[3-endo-(3-hydroxy-phenyl)-8-azabicyclo[3.2.1]oct-8-yl]ethyl}-2-hydroxyacetamide trifluoroacetate

Guidance literature:: 3-endo-[8-(2-amino-3-cyclohexylpropyl)-8-aza-bicyclo[3.2.1]oct-3-yl]phenol; Acetoxyacetyl chloride; With triethylamine; In dichloromethane; for 0.5h;

With methanol; sodium hydroxide; water;