4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)-

Base Information

• Chemical Name: 4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)-
• CAS No.: 103635-24-1
• Molecular Formula: C₁₇H₁₆N₂O₂
• Molecular Weight: 280.326
• Hs Code.: 2928000090
• Mol file: 103635-24-1.mol

Synonyms:Benzoicacid, 4-methoxy-, (3-phenyl-2-propenylidene)hydrazide (9CI)

Chemical Property of 4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)-

Chemical Property:

• PSA: 33.62000
• LogP: 3.87930

Purity/Quality:

4-METHOXY-N'-(3-PHENYL-2-PROPENYLIDENE)BENZOHYDRAZIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)-

There total 2 articles about 4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

→ (E)-4-methoxy-N'-((E)-3-phenylallylidene)benzohydrazide (103635-24-1)

Guidance literature:

In neat (no solvent); for 0.5h; Milling;

Reference yield: 70.0%

4-methoxybenzoic acid hydrazide (3290-99-1) + 3-phenyl-propenal (104-55-2) → PhCHCHCHNNHCO-p-CH3OC6H4 (103635-24-1)

Guidance literature:

In ethanol; for 3h; Heating;

Reference yield:

nickel(II) acetate tetrahydrate (6018-89-9) + PhCHCHCHNNHCO-p-CH3OC6H4 (103635-24-1) → Ni(PhCHCHC(H)N2CO-p-CH3OC6H4)2*2H2O

Guidance literature:

In ethanol; refluxed; 60 min;; cooled; washed with EtOH; air-dried; elem. anal.;;

DOI:10.1016/S0277-5387(00)81669-1

upstream raw materials:

4-methoxybenzoic acid hydrazide

3-phenyl-propenal

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