Methanesulfonic acid (2S,3R,4S)-1-benzyl-4-isopropenyl-2-phenyl-piperidin-3-yl ester

Base Information

Chemical Name:Methanesulfonic acid (2S,3R,4S)-1-benzyl-4-isopropenyl-2-phenyl-piperidin-3-yl ester
CAS No.:190774-39-1
Molecular Formula:C₂₂H₂₇NO₃S
Molecular Weight:385.527
Hs Code.:

Synonyms:Methanesulfonic acid (2S,3R,4S)-1-benzyl-4-isopropenyl-2-phenyl-piperidin-3-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanesulfonic acid (2S,3R,4S)-1-benzyl-4-isopropenyl-2-phenyl-piperidin-3-yl ester

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Technology Process of Methanesulfonic acid (2S,3R,4S)-1-benzyl-4-isopropenyl-2-phenyl-piperidin-3-yl ester

There total 1 articles about Methanesulfonic acid (2S,3R,4S)-1-benzyl-4-isopropenyl-2-phenyl-piperidin-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 124-63-0
methanesulfonyl chloride

: 190774-37-9
(2S,3R,4S)-N-benzyl-3-hydroxy-4-isopropenyl-2-phenylpiperidine

: 190774-39-1
Methanesulfonic acid (2S,3R,4S)-1-benzyl-4-isopropenyl-2-phenyl-piperidin-3-yl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1055/s-1997-1201

Reference yield: 64.0%

: 190774-39-1
Methanesulfonic acid (2S,3R,4S)-1-benzyl-4-isopropenyl-2-phenyl-piperidin-3-yl ester

: 190774-40-4
(2S,3S,4S)-3-azido-N-benzyl-4-isopropenyl-2-phenylpiperidine

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 100 ℃; for 20h;
DOI:10.1055/s-1997-1201

Reference yield:

: 190774-39-1
Methanesulfonic acid (2S,3R,4S)-1-benzyl-4-isopropenyl-2-phenyl-piperidin-3-yl ester

: (2S,3S,4S)-3-amino-N-benzyl-4-isopropenyl-2-phenylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / NaN₃ / dimethylformamide / 20 h / 100 °C

2: 99 percent / H₂ / Pd/C / methanol / 48 h / 760 Torr / Ambient temperature

With sodium azide; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-1997-1201