{C₅H₅(CO)2Mn}2SC₆H₄NO₂⁽¹⁺⁾*PF₆^(1-)*0.5CH₂Cl₂ = {C₅H₅(CO)2Mn}2SC₆H₄NO₂PF₆*0.5CH₂Cl₂

Base Information

• Chemical Name: {C₅H₅(CO)2Mn}2SC₆H₄NO₂⁽¹⁺⁾*PF₆^(1-)*0.5CH₂Cl₂ = {C₅H₅(CO)2Mn}2SC₆H₄NO₂PF₆*0.5CH₂Cl₂
• CAS No.: 136379-20-9
• Molecular Formula: 0CH₂Cl₂*C₂₀H₁₄Mn₂NO₆S*F₆P
• Molecular Weight: 693.707

Synonyms:{C₅H₅(CO)2Mn}2SC₆H₄NO₂⁽¹⁺⁾*PF₆^(1-)*0.5CH₂Cl₂ = {C₅H₅(CO)2Mn}2SC₆H₄NO₂PF₆*0.5CH₂Cl₂

Chemical Property of {C₅H₅(CO)2Mn}2SC₆H₄NO₂⁽¹⁺⁾*PF₆^(1-)*0.5CH₂Cl₂ = {C₅H₅(CO)2Mn}2SC₆H₄NO₂PF₆*0.5CH₂Cl₂

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Technology Process of {C₅H₅(CO)2Mn}2SC₆H₄NO₂⁽¹⁺⁾*PF₆^(1-)*0.5CH₂Cl₂ = {C₅H₅(CO)2Mn}2SC₆H₄NO₂PF₆*0.5CH₂Cl₂

There total 1 articles about {C₅H₅(CO)2Mn}2SC₆H₄NO₂⁽¹⁺⁾*PF₆^(1-)*0.5CH₂Cl₂ = {C₅H₅(CO)2Mn}2SC₆H₄NO₂PF₆*0.5CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

silver(I) hexafluorophosphate (26042-63-7) + C5H5(CO)2MnSC6H4NO2 (136378-96-6) → cymantrene (12079-65-1) + {C5H5(CO)2Mn}2SC6H4NO2(1+)*PF6(1-)*0.5CH2Cl2 = {C5H5(CO)2Mn}2SC6H4NO2PF6*0.5CH2Cl2 (136379-20-9)

Guidance literature:

In toluene; carried out with exclusion of air and moisture; 1 equiv of AgPF6 added to a stirred soln. of the Pd complex; mixt. stirred for further 20 min. at room temp.; volume reduced in vac., pentane added, filtered through silanized silica gel, elution with CH2Cl2, crystn. from CH2Cl2-Et2O (1:1) at -30°C; elem. anal.;

upstream raw materials:

silver(I) hexafluorophosphate

C₅H₅(CO)2MnSC₆H₄NO₂

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