Benzoic acid, 4-ethoxy-2-nitro- (6CI)

Base Information

• Chemical Name: Benzoic acid, 4-ethoxy-2-nitro- (6CI)
• CAS No.: 103440-98-8
• Molecular Formula: C₉H₉NO₅
• Molecular Weight: 211.174
• Hs Code.: 2918990090
• Mol file: 103440-98-8.mol

Synonyms:NSC 509716

Chemical Property of Benzoic acid, 4-ethoxy-2-nitro- (6CI)

Chemical Property:

• Vapor Pressure: 1.92E-06mmHg at 25°C
• Refractive Index: 1.575
• Boiling Point: 379.7°C at 760 mmHg
• Flash Point: 183.5°C
• PSA: 92.35000
• Density: 1.368g/cm³
• LogP: 2.21490

Purity/Quality:

98%min ^*data from raw suppliers

4-Ethoxy-2-nitrobenzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-ethoxy-2-nitro- (6CI)

There total 3 articles about Benzoic acid, 4-ethoxy-2-nitro- (6CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-ethoxy-1-methyl-2-nitrobenzene (102871-92-1) → 4-ethoxy-2-nitro-benzoic acid (103440-98-8)

Guidance literature:

With potassium permanganate;

Reference yield:

4-methyl-5-nitrophenol (2042-14-0) → 4-ethoxy-2-nitro-benzoic acid (103440-98-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous NaOH

2: aqueous KMnO₄

With sodium hydroxide; potassium permanganate;

Reference yield:

4-chloromethyl-3-nitro-phenetole (99839-03-9) + sodium acetate (127-09-3) → 4-ethoxy-2-nitro-benzoic acid (103440-98-8)

Guidance literature:

With methanol; Erhitzen des Reaktionsprodukts mit wss. KMnO₄;

upstream raw materials:

4-ethoxy-1-methyl-2-nitrobenzene

4-chloromethyl-3-nitro-phenetole

sodium acetate

4-methyl-5-nitrophenol