amino>acetaldehyde diethyl acetal

Base Information

• Chemical Name: amino>acetaldehyde diethyl acetal
• CAS No.: 104489-60-3
• Molecular Formula: C₁₄H₂₂N₂O₃
• Molecular Weight: 266.34

Synonyms:amino>acetaldehyde diethyl acetal

Chemical Property of amino>acetaldehyde diethyl acetal

Chemical Property:

Purity/Quality:

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Technology Process of amino>acetaldehyde diethyl acetal

There total 3 articles about amino>acetaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-[(Z)-2,2-Diethoxy-ethylimino]-2-phenyl-acetamide (104489-59-0) → amino>acetaldehyde diethyl acetal (104489-60-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 2h; under 2585.7 Torr;

DOI:10.1021/jm00162a008

Reference yield:

2-oxo-2-phenylacetamide (7505-92-2) → amino>acetaldehyde diethyl acetal (104489-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 53 percent / HOAc / CH₂Cl₂ / 18 h / Ambient temperature

2: 96 percent / H₂ / 5percent Pd/C / ethyl acetate / 2 h / 2585.7 Torr

With hydrogen; acetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;

DOI:10.1021/jm00162a008

Reference yield:

2,2-diethoxy-ethanamine (645-36-3) → amino>acetaldehyde diethyl acetal (104489-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 53 percent / HOAc / CH₂Cl₂ / 18 h / Ambient temperature

2: 96 percent / H₂ / 5percent Pd/C / ethyl acetate / 2 h / 2585.7 Torr

With hydrogen; acetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;

DOI:10.1021/jm00162a008

upstream raw materials:

2-[(Z)-2,2-Diethoxy-ethylimino]-2-phenyl-acetamide

2-oxo-2-phenylacetamide

2,2-diethoxy-ethanamine

Downstream raw materials:

1-(2-amino-1-phenylethyl)imidazole-2-thione

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