(2S,3S)-4-bromo-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]butane-1,3-diyl diethanoate

Base Information

• Chemical Name: (2S,3S)-4-bromo-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]butane-1,3-diyl diethanoate
• CAS No.: 1101134-03-5
• Molecular Formula: C₂₇H₃₇BrO₆Si
• Molecular Weight: 565.577

Synonyms:(2S,3S)-4-bromo-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]butane-1,3-diyl diethanoate

Chemical Property of (2S,3S)-4-bromo-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]butane-1,3-diyl diethanoate

Chemical Property:

Purity/Quality:

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Technology Process of (2S,3S)-4-bromo-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]butane-1,3-diyl diethanoate

There total 1 articles about (2S,3S)-4-bromo-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]butane-1,3-diyl diethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetyl bromide (506-96-7) + C23H34O5Si (1101134-02-4) → (2S,3S)-4-bromo-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]butane-1,3-diyl diethanoate (1101134-03-5)

Guidance literature:

C₂₃H₃₄O₅Si; With Trimethyl orthoacetate; pyridinium p-toluenesulfonate; In dichloromethane; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

Acetyl bromide; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.tet.2010.05.028

Reference yield: 99.0%

(2S,3S)-4-bromo-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]butane-1,3-diyl diethanoate (1101134-03-5) → C23H32O4Si (1101134-04-6)

Guidance literature:

With methanol; potassium carbonate; at 0 - 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1016/j.tet.2010.05.028

upstream raw materials:

Acetyl bromide

C₂₃H₃₄O₅Si

Downstream raw materials:

C₂₃H₃₂O₄Si

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