1-O-(2-O-benzoyl-3,5-di-O-benzyl-α-D-arabinofuranosyl) trichloroacetimidate

Base Information

Chemical Name:1-O-(2-O-benzoyl-3,5-di-O-benzyl-α-D-arabinofuranosyl) trichloroacetimidate
CAS No.:915149-97-2
Molecular Formula:C₂₈H₂₆Cl₃NO₆
Molecular Weight:578.877
Hs Code.:

Synonyms:1-O-(2-O-benzoyl-3,5-di-O-benzyl-α-D-arabinofuranosyl) trichloroacetimidate

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Chemical Property of 1-O-(2-O-benzoyl-3,5-di-O-benzyl-α-D-arabinofuranosyl) trichloroacetimidate

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Technology Process of 1-O-(2-O-benzoyl-3,5-di-O-benzyl-α-D-arabinofuranosyl) trichloroacetimidate

There total 5 articles about 1-O-(2-O-benzoyl-3,5-di-O-benzyl-α-D-arabinofuranosyl) trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1,2-O-(α-allyloxybenzylidene)-β-D-arabinofuranose

: 915149-97-2
1-O-(2-O-benzoyl-3,5-di-O-benzyl-α-D-arabinofuranosyl) trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NaH / dimethylformamide / 0 - 20 °C

2: p-toluenesulfonic acid / H₂O; 1,2-dimethoxy-ethane / 2 h / 0 - 20 °C

3: 3.71 g / DBU / CH₂Cl₂ / 0.5 h / 0 °C

With sodium hydride; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo061233x

Reference yield:

: C₂₆H₂₁ClO₇

: 915149-97-2
1-O-(2-O-benzoyl-3,5-di-O-benzyl-α-D-arabinofuranosyl) trichloroacetimidate

Guidance literature:: Multi-step reaction with 5 steps

1: 10.4 g / 2,6-lutidine / CH₂Cl₂ / 18 h / 20 °C

2: 4.85 g / NaOMe / methanol / 48 h / 20 °C

3: 95 percent / NaH / dimethylformamide / 0 - 20 °C

4: p-toluenesulfonic acid / H₂O; 1,2-dimethoxy-ethane / 2 h / 0 - 20 °C

5: 3.71 g / DBU / CH₂Cl₂ / 0.5 h / 0 °C

With 2,6-dimethylpyridine; sodium methylate; sodium hydride; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo061233x

Reference yield:

: 1,2-O-(α-allyloxybenzylidene)-3,5-di-O-benzyl-β-D-arabinofuranose

: 915149-97-2
1-O-(2-O-benzoyl-3,5-di-O-benzyl-α-D-arabinofuranosyl) trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid / H₂O; 1,2-dimethoxy-ethane / 2 h / 0 - 20 °C

2: 3.71 g / DBU / CH₂Cl₂ / 0.5 h / 0 °C

With toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1021/jo061233x