12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C

Base Information

Chemical Name:12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C
CAS No.:223716-95-8
Molecular Formula:C₂₈H₃₇NO₃
Molecular Weight:436.596
Hs Code.:

Synonyms:12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C

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Technology Process of 12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C

There total 1 articles about 12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 25909-68-6
[¹³C]-potassium cyanide

: 223716-93-6
11-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]undecyl bromide

: 223716-95-8
12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C

Guidance literature:: With 18-crown-6 ether; In acetonitrile; for 9h; Heating;
DOI:10.1246/bcsj.72.347

Reference yield: 66.0%

: 223716-95-8
12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C

: 223716-96-9
12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid

Guidance literature:: With potassium hydroxide; In ethanol; water; for 22h; Heating;
DOI:10.1246/bcsj.72.347

Reference yield:

: 223716-95-8
12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C

: p-(12-anilinododecyl-12-13C-oxy)benzophenone

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / KOH / ethanol; H₂O / 22 h / Heating

2: 96 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 2 h / Heating

3: lithium aluminum hydride / tetrahydrofuran / 7 h / Heating

4: 117 mg / aq. HCl / methanol / 0.5 h

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1: Hydrolysis / 2: Acylation / 3: Reduction / 4: Hydrolysis;
DOI:10.1246/bcsj.72.347