12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid

Base Information

Chemical Name:12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid
CAS No.:223716-96-9
Molecular Formula:C₂₈H₃₈O₅
Molecular Weight:455.596
Hs Code.:

Synonyms:12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid

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Chemical Property of 12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid

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Technology Process of 12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid

There total 1 articles about 12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 223716-95-8
12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanenitrile-1-13C

: 223716-96-9
12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid

Guidance literature:: With potassium hydroxide; In ethanol; water; for 22h; Heating;
DOI:10.1246/bcsj.72.347

Reference yield: 96.0%

: 62-53-3
aniline

: 223716-96-9
12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid

: 223716-98-1
C₃₃⁽¹³⁾CH₄₃NO₄

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 2h; Heating;
DOI:10.1246/bcsj.72.347

Reference yield:

: 223716-96-9
12-[p-(4-methyl-2-phenyl-1,3-dioxolan-2-yl)phenoxy]dodecanoic-1-13C acid

: p-(12-anilinododecyl-12-13C-oxy)benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 2 h / Heating

2: lithium aluminum hydride / tetrahydrofuran / 7 h / Heating

3: 117 mg / aq. HCl / methanol / 0.5 h

With hydrogenchloride; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; 1: Acylation / 2: Reduction / 3: Hydrolysis;
DOI:10.1246/bcsj.72.347