(S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline

Base Information

Chemical Name:(S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline
CAS No.:32886-69-4
Molecular Formula:C₂₀H₂₅NO₅
Molecular Weight:359.422
Hs Code.:

Synonyms:(S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline

Suppliers and Price of (S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline

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Technology Process of (S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline

There total 11 articles about (S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (R)-2-[(S)-6,7-Dimethoxy-1-(3,4,5-trimethoxy-phenyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-phenyl-ethanol

: 32886-69-4
(S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; for 8h; Ambient temperature;
DOI:10.1016/0040-4039(96)00819-2

Reference yield: 58.0%

: 1242161-97-2
(1S)-6,7-dimethoxy-3-oxo-1-[3,4,5-(trimethoxyphenyl)]-1,2,3,4-tetrahydroisoquinoline

: 32886-69-4
(S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline

Guidance literature:: With sodium tetrahydroborate; iodine; In tetrahydrofuran; at 0 ℃; Reflux;
DOI:10.1002/ejoc.201000473

Reference yield:

: 3161-21-5
1-(3,4,5-trimethoxylphenyl)-3,4-dihydro-6,7-dimethoxyisoquinoline

: 32886-70-7
6,7-dimethoxy-1-(3,4,5-trimethoxyphenyl)-1,2,3,4-tetrahydroisoquinoline

: 32886-69-4
(S)-1-(3',4',5'-trimethoxylphenyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₄₂H₄₆FeP₂; hydrogen bromide; hydrogen; In tetrahydrofuran; water; at 30 ℃; for 12h; under 38002.6 Torr; Overall yield = 99 percent; Overall yield = 177.7 mg; enantioselective reaction; Schlenk technique; Autoclave;
DOI:10.1021/acs.orglett.9b03251