4-(2-(3-chloro-4-methoxyphenyl)-4,5-dihydroimidazol-1-yl)benzenesulfonamide

Base Information

Chemical Name:4-(2-(3-chloro-4-methoxyphenyl)-4,5-dihydroimidazol-1-yl)benzenesulfonamide
CAS No.:1621586-83-1
Molecular Formula:C₁₆H₁₆ClN₃O₃S
Molecular Weight:365.84
Hs Code.:

Synonyms:4-(2-(3-chloro-4-methoxyphenyl)-4,5-dihydroimidazol-1-yl)benzenesulfonamide

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Chemical Property of 4-(2-(3-chloro-4-methoxyphenyl)-4,5-dihydroimidazol-1-yl)benzenesulfonamide

Chemical Property:

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Technology Process of 4-(2-(3-chloro-4-methoxyphenyl)-4,5-dihydroimidazol-1-yl)benzenesulfonamide

There total 4 articles about 4-(2-(3-chloro-4-methoxyphenyl)-4,5-dihydroimidazol-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₃₆ClN₃O₇S

: 1621586-83-1
4-(2-(3-chloro-4-methoxyphenyl)-4,5-dihydroimidazol-1-yl)benzenesulfonamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃;
DOI:10.1016/j.ejmech.2014.07.023

Reference yield:

: 4903-09-7
3-chloro-4-methoxy-benzaldehyde

: 1621586-83-1
4-(2-(3-chloro-4-methoxyphenyl)-4,5-dihydroimidazol-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 0.33 h / 0 °C

1.2: 12 h / 0 - 20 °C

2.1: caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20 h / Sealed tube; Inert atmosphere; Heating

3.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1080/14756366.2016.1178248

Reference yield:

: 1375748-31-4
2-(3-chloro-4-methoxyphenyl)-4,5-dihydro-1H-imidazole

: 1621586-83-1
4-(2-(3-chloro-4-methoxyphenyl)-4,5-dihydroimidazol-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20 h / Sealed tube; Inert atmosphere; Heating

2: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1080/14756366.2016.1178248