C₃₀H₃₀Cl₃NO₅

Base Information

• Chemical Name: C₃₀H₃₀Cl₃NO₅
• CAS No.: 1101117-89-8
• Molecular Formula: C₃₀H₃₀Cl₃NO₅
• Molecular Weight: 590.931
• Mol file: 1101117-89-8.mol

Synonyms:C₃₀H₃₀Cl₃NO₅

Chemical Property of C₃₀H₃₀Cl₃NO₅

Chemical Property:

Purity/Quality:

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Technology Process of C₃₀H₃₀Cl₃NO₅

There total 1 articles about C₃₀H₃₀Cl₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide (1101117-87-6) → C30H30Cl3NO5 (1101117-89-8)

Guidance literature:

N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; tert-butyl alcohol; at 20 ℃; for 3h;

With sodium disulfite; In water; acetone; tert-butyl alcohol; for 0.166667h; regioselective reaction;

DOI:10.1039/b810654a

Reference yield: 91.5%

C30H30Cl3NO5 (1101117-89-8) → 2,2,2-trichloro-N-((2S,3S,6R)-6-(2-oxoethyl)-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)acetamide (1101117-88-7)

Guidance literature:

With sodium periodate; In methanol; water; at 0 ℃; for 0.5h;

DOI:10.1039/b810654a

upstream raw materials:

N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide

Downstream raw materials:

2,2,2-trichloro-N-((2S,3S,6R)-6-(2-oxoethyl)-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)acetamide