10,10-Dimethyl-9-phenyl-7,8,11,12-tetraaza-tricyclo[7.2.1.0^1,6]dodec-6-ene-11,12-diol

Base Information

• Chemical Name: 10,10-Dimethyl-9-phenyl-7,8,11,12-tetraaza-tricyclo[7.2.1.0^1,6]dodec-6-ene-11,12-diol
• CAS No.: 82811-34-5
• Molecular Formula: C₁₆H₂₂N₄O₂
• Molecular Weight: 302.376

Synonyms:10,10-Dimethyl-9-phenyl-7,8,11,12-tetraaza-tricyclo[7.2.1.0^1,6]dodec-6-ene-11,12-diol

Chemical Property of 10,10-Dimethyl-9-phenyl-7,8,11,12-tetraaza-tricyclo[7.2.1.0^1,6]dodec-6-ene-11,12-diol

Chemical Property:

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Technology Process of 10,10-Dimethyl-9-phenyl-7,8,11,12-tetraaza-tricyclo[7.2.1.0^1,6]dodec-6-ene-11,12-diol

There total 3 articles about 10,10-Dimethyl-9-phenyl-7,8,11,12-tetraaza-tricyclo[7.2.1.0^1,6]dodec-6-ene-11,12-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

5,5-dimethyl-1-hydroxy-2-(spirocyclohexan-2-one 2)-4-phenyl-3-imidazoline 3-oxide (82811-27-6) → 10,10-Dimethyl-9-phenyl-7,8,11,12-tetraaza-tricyclo[7.2.1.01,6]dodec-6-ene-11,12-diol (82811-34-5)

Guidance literature:

With hydrazine hydrate; In ethanol; for 10h;

DOI:10.1007/BF00949952

Reference yield:

N-(2-methyl-1-oximino-1-phenyl-2-propyl)hydroxylamine (5291-08-7) → 10,10-Dimethyl-9-phenyl-7,8,11,12-tetraaza-tricyclo[7.2.1.01,6]dodec-6-ene-11,12-diol (82811-34-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / methanol / 6 h / Heating

2: 98 percent / hydrazine hydrate / ethanol / 10 h

With hydrazine hydrate; In methanol; ethanol;

DOI:10.1007/BF00949952

Reference yield:

cyclohexane-1,2-dione (765-87-7) → 10,10-Dimethyl-9-phenyl-7,8,11,12-tetraaza-tricyclo[7.2.1.01,6]dodec-6-ene-11,12-diol (82811-34-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / methanol / 6 h / Heating

2: 98 percent / hydrazine hydrate / ethanol / 10 h

With hydrazine hydrate; In methanol; ethanol;

DOI:10.1007/BF00949952

upstream raw materials:

5,5-dimethyl-1-hydroxy-2-(spirocyclohexan-2-one 2)-4-phenyl-3-imidazoline 3-oxide

N-(2-methyl-1-oximino-1-phenyl-2-propyl)hydroxylamine

cyclohexane-1,2-dione

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