PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NCl⁽¹⁺⁾*ClO₄^(1-)=PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NClClO₄

Base Information

• Chemical Name: PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NCl⁽¹⁺⁾*ClO₄^(1-)=PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NClClO₄
• CAS No.: 92391-87-2
• Molecular Formula: C₂₂H₂₈Cl₂NP₂Pd*ClO₄
• Molecular Weight: 645.195

Synonyms:PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NCl⁽¹⁺⁾*ClO₄^(1-)=PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NClClO₄

Chemical Property of PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NCl⁽¹⁺⁾*ClO₄^(1-)=PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NClClO₄

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Technology Process of PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NCl⁽¹⁺⁾*ClO₄^(1-)=PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NClClO₄

There total 3 articles about PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NCl⁽¹⁺⁾*ClO₄^(1-)=PdCl(P(C₆H₅(CH₃)2))2C₅H₃CH₃NClClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

PdCl(P(C6H5)3)2C5H3NCH3Cl(1+)*ClO4(1-)=(PdCl(P(C6H5)3)2C5H3NCH3Cl)ClO4 (92391-83-8) + Dimethyl(phenyl)phosphine (672-66-2) → PdCl(P(C6H5(CH3)2))2C5H3CH3NCl(1+)*ClO4(1-)=PdCl(P(C6H5(CH3)2))2C5H3CH3NClClO4 (92391-87-2)

Guidance literature:

In dichloromethane; under N2; stirring for 30 min at room temp.;; treatment with charcoal; filtn.; concn.; pptn. with diethyl ether; elem. anal.;;

DOI:10.1016/0022-328X(84)80316-2

Reference yield:

2,6-dichloropyridine (2402-78-0) → PdCl(P(C6H5(CH3)2))2C5H3CH3NCl(1+)*ClO4(1-)=PdCl(P(C6H5(CH3)2))2C5H3CH3NClClO4 (92391-87-2)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene

2: dichloromethane

3: dichloromethane

In dichloromethane; toluene;

DOI:10.1016/0022-328X(84)80316-2

Reference yield:

(ClPd(P(C6H5)3)2C5H3ClN) → PdCl(P(C6H5(CH3)2))2C5H3CH3NCl(1+)*ClO4(1-)=PdCl(P(C6H5(CH3)2))2C5H3CH3NClClO4 (92391-87-2)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: dichloromethane

In dichloromethane;

DOI:10.1016/0022-328X(84)80316-2

upstream raw materials:

PdCl(P(C₆H₅)3)2C₅H₃NCH₃Cl⁽¹⁺⁾*ClO₄^(1-)=(PdCl(P(C₆H₅)3)2C₅H₃NCH₃Cl)ClO₄

Dimethyl(phenyl)phosphine

2,6-dichloropyridine

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