(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid

Base Information

Chemical Name:(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid
CAS No.:1265819-92-8
Molecular Formula:C₁₅H₁₉ClO₄S
Molecular Weight:330.832
Hs Code.:

Synonyms:(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid

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Chemical Property of (S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid

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Technology Process of (S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid

There total 2 articles about (S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 345635-33-8
(E)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-acrylic acid

: 300356-14-3
(R)-2-(3-chloro-4-(methylsulfonyl)phenyl)-3-cyclopentylpropanoic acid

: 1265819-92-8
(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid

Guidance literature:: With hydrogen; [(S)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-dimethylphenyl)-phosphineo]bisacetato]ruthenium(II); In methanol; at 50 ℃; for 17h; under 37503.8 Torr; Product distribution / selectivity; Autoclave;

Reference yield:

: 87776-75-8
(3-chloro-4-methylsulfanyl-phenyl)-acetic acid

: 300356-14-3
(R)-2-(3-chloro-4-(methylsulfonyl)phenyl)-3-cyclopentylpropanoic acid

: 1265819-92-8
(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: formic acid; dihydrogen peroxide / water / 16 h / 50 °C

2.1: acetic anhydride; sodium acetate / tetrahydrofuran / 24 h / 40 °C

2.2: 2 h / 40 °C

2.3: pH 6

3.1: hydrogen / [(S)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-dimethylphenyl)-phosphineo]bisacetato]ruthenium(II) / methanol / 17 h / 50 °C / 37503.8 Torr / Autoclave

With formic acid; hydrogen; dihydrogen peroxide; sodium acetate; acetic anhydride; [(S)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-dimethylphenyl)-phosphineo]bisacetato]ruthenium(II); In tetrahydrofuran; methanol; water;