ethyl 2-(4-{2-[N-(heptyl)-N-(benzoxazol-2-yl)amino]ethyl}phenoxy)ethanoate

Base Information

Chemical Name:ethyl 2-(4-{2-[N-(heptyl)-N-(benzoxazol-2-yl)amino]ethyl}phenoxy)ethanoate
CAS No.:1350846-87-5
Molecular Formula:C₂₆H₃₄N₂O₄
Molecular Weight:438.567
Hs Code.:

Synonyms:ethyl 2-(4-{2-[N-(heptyl)-N-(benzoxazol-2-yl)amino]ethyl}phenoxy)ethanoate

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Chemical Property of ethyl 2-(4-{2-[N-(heptyl)-N-(benzoxazol-2-yl)amino]ethyl}phenoxy)ethanoate

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Technology Process of ethyl 2-(4-{2-[N-(heptyl)-N-(benzoxazol-2-yl)amino]ethyl}phenoxy)ethanoate

There total 6 articles about ethyl 2-(4-{2-[N-(heptyl)-N-(benzoxazol-2-yl)amino]ethyl}phenoxy)ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 198756-78-4
C₂₀H₂₃NO₅

: 1350846-87-5
ethyl 2-(4-{2-[N-(heptyl)-N-(benzoxazol-2-yl)amino]ethyl}phenoxy)ethanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol / 1.5 h / 20 °C / 3800.26 Torr

2.1: benzotriazol-1-ol; diisopropyl-carbodiimide / dichloromethane / 15 h / 20 °C

3.1: borane-THF / tetrahydrofuran / 20 °C / Inert atmosphere

3.2: 0.5 h / Reflux; Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 18 h / 0 °C / Reflux

With borane-THF; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; triethylamine; diisopropyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm201306q

Reference yield:

: 1350846-83-1
ethyl 2-[4-(2-heptanoylaminoethyl)phenoxy]ethanoate

: 1350846-87-5
ethyl 2-(4-{2-[N-(heptyl)-N-(benzoxazol-2-yl)amino]ethyl}phenoxy)ethanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane-THF / tetrahydrofuran / 20 °C / Inert atmosphere

1.2: 0.5 h / Reflux; Inert atmosphere

2.1: triethylamine / tetrahydrofuran / 18 h / 0 °C / Reflux

With borane-THF; triethylamine; In tetrahydrofuran;
DOI:10.1021/jm201306q

Reference yield:

: 72131-30-7
ethyl 2-(4-(2-aminoethyl)phenoxy)acetate

: 1350846-87-5
ethyl 2-(4-{2-[N-(heptyl)-N-(benzoxazol-2-yl)amino]ethyl}phenoxy)ethanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; diisopropyl-carbodiimide / dichloromethane / 15 h / 20 °C

2.1: borane-THF / tetrahydrofuran / 20 °C / Inert atmosphere

2.2: 0.5 h / Reflux; Inert atmosphere

3.1: triethylamine / tetrahydrofuran / 18 h / 0 °C / Reflux

With borane-THF; benzotriazol-1-ol; triethylamine; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm201306q