(S,S)-1-benzyl-3-(2-methoxycarbonylamino-3-methylbutyryl)imidazolidine-4-carboxlic acid methyl ester

Base Information

Chemical Name:(S,S)-1-benzyl-3-(2-methoxycarbonylamino-3-methylbutyryl)imidazolidine-4-carboxlic acid methyl ester
CAS No.:1256386-93-2
Molecular Formula:C₁₉H₂₇N₃O₅
Molecular Weight:377.44
Hs Code.:

Synonyms:(S,S)-1-benzyl-3-(2-methoxycarbonylamino-3-methylbutyryl)imidazolidine-4-carboxlic acid methyl ester

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Chemical Property of (S,S)-1-benzyl-3-(2-methoxycarbonylamino-3-methylbutyryl)imidazolidine-4-carboxlic acid methyl ester

Chemical Property:

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Technology Process of (S,S)-1-benzyl-3-(2-methoxycarbonylamino-3-methylbutyryl)imidazolidine-4-carboxlic acid methyl ester

There total 3 articles about (S,S)-1-benzyl-3-(2-methoxycarbonylamino-3-methylbutyryl)imidazolidine-4-carboxlic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1256386-92-1
(S)-1-benzylimidazolidine-4-carboxlic acid methyl ester

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1256386-93-2
(S,S)-1-benzyl-3-(2-methoxycarbonylamino-3-methylbutyryl)imidazolidine-4-carboxlic acid methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 1256386-91-0
(S)-methyl 3-(benzylamino)-2-(tert-butoxycarbonylamino)propanoate

: 1256386-93-2
(S,S)-1-benzyl-3-(2-methoxycarbonylamino-3-methylbutyryl)imidazolidine-4-carboxlic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane; dichloromethane / 0.5 h / 20 °C

1.2: 48 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: sodium (S)-3-benzylamino-2-tert-butoxycarbonylaminopropioate

: 1256386-93-2
(S,S)-1-benzyl-3-(2-methoxycarbonylamino-3-methylbutyryl)imidazolidine-4-carboxlic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / water

1.2: 0 - 20 °C

2.1: hydrogenchloride / 1,4-dioxane; dichloromethane / 0.5 h / 20 °C

2.2: 48 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;