sodium 1-(5-chloro-2-((4-chloro-2-fluorobenzyl)oxy)benzyl)-1,2,3,4-tetrahydroquinoline-5-sulfonate

Base Information

Chemical Name:sodium 1-(5-chloro-2-((4-chloro-2-fluorobenzyl)oxy)benzyl)-1,2,3,4-tetrahydroquinoline-5-sulfonate
CAS No.:1428128-19-1
Molecular Formula:C₂₃H₁₉Cl₂FNO₄S*Na
Molecular Weight:518.368
Hs Code.:

Synonyms:sodium 1-(5-chloro-2-((4-chloro-2-fluorobenzyl)oxy)benzyl)-1,2,3,4-tetrahydroquinoline-5-sulfonate

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Chemical Property of sodium 1-(5-chloro-2-((4-chloro-2-fluorobenzyl)oxy)benzyl)-1,2,3,4-tetrahydroquinoline-5-sulfonate

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Technology Process of sodium 1-(5-chloro-2-((4-chloro-2-fluorobenzyl)oxy)benzyl)-1,2,3,4-tetrahydroquinoline-5-sulfonate

There total 4 articles about sodium 1-(5-chloro-2-((4-chloro-2-fluorobenzyl)oxy)benzyl)-1,2,3,4-tetrahydroquinoline-5-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427422-74-9
2-(bromomethyl)-4-chloro-1-((4-chloro-2-fluorobenzyl)oxy)benzene

: 1428129-17-2
sodium 1,2,3,4-tetrahydroquinoline-5-sulfonate

: 1428128-19-1
sodium 1-(5-chloro-2-((4-chloro-2-fluorobenzyl)oxy)benzyl)-1,2,3,4-tetrahydroquinoline-5-sulfonate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 102878-84-2
quinoline-5-sulfonyl chloride

: 1428128-19-1
sodium 1-(5-chloro-2-((4-chloro-2-fluorobenzyl)oxy)benzyl)-1,2,3,4-tetrahydroquinoline-5-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; sodium hydroxide / 1,4-dioxane; water / 3 h / 60 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With dmap; palladium 10% on activated carbon; hydrogen; potassium carbonate; sodium hydroxide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 23261-58-7
quinoline-5-sulfonic acid

: 1428128-19-1
sodium 1-(5-chloro-2-((4-chloro-2-fluorobenzyl)oxy)benzyl)-1,2,3,4-tetrahydroquinoline-5-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In methanol; N,N-dimethyl-formamide;