C₄₂H₆₀N₈O₁₂S₂

Base Information

Chemical Name:C₄₂H₆₀N₈O₁₂S₂
CAS No.:952715-79-6
Molecular Formula:C₄₂H₆₀N₈O₁₂S₂
Molecular Weight:933.117
Hs Code.:

C<sub>42</sub>H<sub>60</sub>N<sub>8</sub>O<sub>12</sub>S<sub>2</sub>

Synonyms:C₄₂H₆₀N₈O₁₂S₂

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Chemical Property of C₄₂H₆₀N₈O₁₂S₂

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Technology Process of C₄₂H₆₀N₈O₁₂S₂

There total 1 articles about C₄₂H₆₀N₈O₁₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 4331-98-0
cyanogen di-N-oxide

: 952658-49-0
1,2-bis(2-{4'-[4'-(methylphenyl)sulfonyl]-1',7'-dioxa-4',10'-diazacyclododecane}ethoxy)-4,5-diaminobenzene

: 952715-79-6
C₄₂H₆₀N₈O₁₂S₂

Guidance literature:: With sodium carbonate; In dichloromethane; water; at -10 ℃; for 18h;
DOI:10.1246/bcsj.80.1549

Reference yield: 84.0%

: nickel(II) chloride hexahydrate

: 952715-79-6
(CH₃C₆H₄SO₂N(CH₂CH₂OCH₂CH₂)2NCH₂CH₂O)2C₆H₂N₂H₂C₂(NOH)2

: ((CH₃C₆H₄SO₂N(CH₂CH₂OCH₂CH₂)2NCH₂CH₂O)2C₆H₂N₂H₂C₂(NO)NOH)2Ni

Guidance literature:: With triethylamine; In ethanol; soln. of Ni salt in EtOH added to soln. of ligand in EtOH at 60°C; EtOH soln. of Et3N added under heating (60°C) and stirring, pH 4.5-5.0; heated in water bath for 2 h; filtered; ppt. washed with H2O, EtOH and Et2O; dried in vac. over P2O5; elem. anal.;
DOI:10.1246/bcsj.80.1549

Reference yield: 76.0%

: copper(II) choride dihydrate

: 952715-79-6
(CH₃C₆H₄SO₂N(CH₂CH₂OCH₂CH₂)2NCH₂CH₂O)2C₆H₂N₂H₂C₂(NOH)2

: ((CH₃C₆H₄SO₂N(CH₂CH₂OCH₂CH₂)2NCH₂CH₂O)2C₆H₂N₂H₂C₂(NO)NOH)2Cu

Guidance literature:: With triethylamine; In ethanol; soln. of Cu salt in EtOH added to soln. of ligand in EtOH at 60°C; EtOH soln. of Et3N added under heating (60°C) and stirring, pH 5.0-6.0; heated in water bath for 2 h; filtered; ppt. washed with H2O, EtOH and Et2O; dried in vac. over P2O5; elem. anal.;
DOI:10.1246/bcsj.80.1549