tert-butyl (S)-1-(4-(1-benzhydrylazetidin-3-yl-oxy)phenyl)ethylcarbamate

Base Information

Chemical Name:tert-butyl (S)-1-(4-(1-benzhydrylazetidin-3-yl-oxy)phenyl)ethylcarbamate
CAS No.:1443670-39-0
Molecular Formula:C₂₉H₃₄N₂O₃
Molecular Weight:458.601
Hs Code.:

Synonyms:tert-butyl (S)-1-(4-(1-benzhydrylazetidin-3-yl-oxy)phenyl)ethylcarbamate

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Chemical Property of tert-butyl (S)-1-(4-(1-benzhydrylazetidin-3-yl-oxy)phenyl)ethylcarbamate

Chemical Property:

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Technology Process of tert-butyl (S)-1-(4-(1-benzhydrylazetidin-3-yl-oxy)phenyl)ethylcarbamate

There total 3 articles about tert-butyl (S)-1-(4-(1-benzhydrylazetidin-3-yl-oxy)phenyl)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931093-42-4
(S)-tert-butyl 1-(4-hydroxyphenyl)ethylcarbamate

: 33301-41-6
1-benzhydryl-3-azetidinyl methanesulfonate

: 1443670-39-0
tert-butyl (S)-1-(4-(1-benzhydrylazetidin-3-yl-oxy)phenyl)ethylcarbamate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 3h;

Reference yield:

: 6298-96-0,22038-86-4,35600-82-9,41851-59-6
(S)-1-(4-methoxyphenyl)ethylamine

: 1443670-39-0
tert-butyl (S)-1-(4-(1-benzhydrylazetidin-3-yl-oxy)phenyl)ethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen bromide; acetic acid / 4 h / 100 °C

2: sodium carbonate / dichloromethane; water / 2 h / 20 °C

3: caesium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

With hydrogen bromide; sodium carbonate; caesium carbonate; acetic acid; In dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1001094-89-8
(S)-4-(1-amino-ethyl)-phenol hydrobromid

: 1443670-39-0
tert-butyl (S)-1-(4-(1-benzhydrylazetidin-3-yl-oxy)phenyl)ethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / dichloromethane; water / 2 h / 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

With sodium carbonate; caesium carbonate; In dichloromethane; water; N,N-dimethyl-formamide;