3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

Base Information

Chemical Name:3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine
CAS No.:61089-03-0
Molecular Formula:C₃₄H₂₈F₁₂N₆O₁₆
Molecular Weight:1004.61
Hs Code.:

Synonyms:3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

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Chemical Property of 3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

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Technology Process of 3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

There total 6 articles about 3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.7%

: 61066-06-6
5,6-O-isopropylidene-3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

: 61089-03-0
3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

Guidance literature:: With acetic acid; at 65 ℃; for 4h;
DOI:10.1021/jm00144a023

Reference yield:

: 3947-65-7
neomycin A

: 61089-03-0
3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

Guidance literature:: Multi-step reaction with 4 steps

1: 75.3 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

2: 76.3 percent / CF₃COOH / acetonitrile / 0.75 h / Heating

3: 94.2 percent / pyridine / 2.5 h / Ambient temperature

4: 80.7 percent / 66percent aq. HOAc / 4 h / 65 °C

With pyridine; acetic acid; triethylamine; trifluoroacetic acid; In acetonitrile;
DOI:10.1021/jm00144a023

Reference yield:

: 61066-03-3
1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

: 61089-03-0
3',4'-bis-O-(p-nitrobenzoyl)-1,2',3,6'-tetrakis-N-(trifluoroacetyl)neamine

Guidance literature:: Multi-step reaction with 3 steps

1: 76.3 percent / CF₃COOH / acetonitrile / 0.75 h / Heating

2: 94.2 percent / pyridine / 2.5 h / Ambient temperature

3: 80.7 percent / 66percent aq. HOAc / 4 h / 65 °C

With pyridine; acetic acid; trifluoroacetic acid; In acetonitrile;
DOI:10.1021/jm00144a023