2-(N-hexyl(3-(((perfluorobutyl)sulfonyl)oxy)phenyl)amino)-2-oxoethyl acetate

Base Information

• Chemical Name: 2-(N-hexyl(3-(((perfluorobutyl)sulfonyl)oxy)phenyl)amino)-2-oxoethyl acetate
• CAS No.: 1407187-89-6
• Molecular Formula: C₂₀H₂₂F₉NO₆S
• Molecular Weight: 575.449

Synonyms:2-(N-hexyl(3-(((perfluorobutyl)sulfonyl)oxy)phenyl)amino)-2-oxoethyl acetate

Chemical Property of 2-(N-hexyl(3-(((perfluorobutyl)sulfonyl)oxy)phenyl)amino)-2-oxoethyl acetate

Chemical Property:

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Technology Process of 2-(N-hexyl(3-(((perfluorobutyl)sulfonyl)oxy)phenyl)amino)-2-oxoethyl acetate

There total 2 articles about 2-(N-hexyl(3-(((perfluorobutyl)sulfonyl)oxy)phenyl)amino)-2-oxoethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

3-(hexylamino)phenyl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate (1407187-87-4) + Acetoxyacetyl chloride (13831-31-7) → 2-(N-hexyl(3-(((perfluorobutyl)sulfonyl)oxy)phenyl)amino)-2-oxoethyl acetate (1407187-89-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol302748h

Reference yield:

recorcinol (108-46-3) → 2-(N-hexyl(3-(((perfluorobutyl)sulfonyl)oxy)phenyl)amino)-2-oxoethyl acetate (1407187-89-6)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

2: palladium diacetate; 4a,9a-dihydro-9,9-dimethyl-4,5-bis(diphenylphosphino)-xanthene; potassium phosphate; toluene / 24 h / 110 °C / Inert atmosphere

3: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With potassium phosphate; 4a,9a-dihydro-9,9-dimethyl-4,5-bis(diphenylphosphino)-xanthene; palladium diacetate; triethylamine; toluene; In dichloromethane;

DOI:10.1021/ol302748h

Reference yield: 95.0%

2-(N-hexyl(3-(((perfluorobutyl)sulfonyl)oxy)phenyl)amino)-2-oxoethyl acetate (1407187-89-6) → 3-(N-hexyl-2-hydroxyacetamido)phenyl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate (1407187-90-9)

Guidance literature:

With potassium carbonate; In methanol; water; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol302748h

upstream raw materials:

3-(hexylamino)phenyl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Acetoxyacetyl chloride

recorcinol

Downstream raw materials:

3-(N-hexyl-2-hydroxyacetamido)phenyl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

3-(2-(bromomethyl)-3,6-dimethylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

C₁₈H₁₈F₉NO₅S

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