C₂₂H₁₉NOS

Base Information

• Chemical Name: C₂₂H₁₉NOS
• CAS No.: 352563-77-0
• Molecular Formula: C₂₂H₁₉NOS
• Molecular Weight: 345.465
• Mol file: 352563-77-0.mol

Synonyms:C₂₂H₁₉NOS

Chemical Property of C₂₂H₁₉NOS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₁₉NOS

There total 1 articles about C₂₂H₁₉NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,2-diphenylthioacetamide (17518-50-2) + α-bromoacetophenone (70-11-1) → C22H19NOS (352563-77-0)

Guidance literature:

With triethylamine; In acetone; at 20 ℃; for 0.5h;

DOI:10.1007/s11172-007-0219-5

Reference yield: 83.0%

C22H19NOS (352563-77-0) → C22H17NS (380171-53-9)

Guidance literature:

With hydrogenchloride; In isopropyl alcohol; for 0.0166667h; Heating;

DOI:10.1007/s11172-007-0219-5

Reference yield: 51.0%

C22H19NOS (352563-77-0) → C22H17NS (1075693-18-3)

Guidance literature:

With acetic acid; In 1,4-dioxane; at 20 ℃; for 12h;

DOI:10.1007/s11172-007-0220-z

upstream raw materials:

2,2-diphenylthioacetamide

α-bromoacetophenone

Downstream raw materials:

C₂₂H₁₇NS

C₂₂H₁₇NS

Refernces