Benzyl (4RS)-(E)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate

Base Information

Chemical Name:Benzyl (4RS)-(E)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate
CAS No.:134676-38-3
Molecular Formula:C₂₈H₃₂N₂O₆
Molecular Weight:492.572
Hs Code.:

Synonyms:Benzyl (4RS)-(E)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate

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Chemical Property of Benzyl (4RS)-(E)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate

Chemical Property:

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Technology Process of Benzyl (4RS)-(E)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate

There total 3 articles about Benzyl (4RS)-(E)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134676-36-1,1267551-72-3
(2-Hydroxy-but-3-enyl)-carbamic acid tert-butyl ester

: 134676-38-3
Benzyl (4RS)-(E)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: 1.) NMO, NaIO₄ / 1.) OsO₄

With sodium periodate; N-methyl-2-indolinone; osmium(VIII) oxide; In pyridine;
DOI:10.1016/S0040-4039(00)95477-7

Reference yield:

: 134676-37-2
Acetic acid 1-(tert-butoxycarbonylamino-methyl)-allyl ester

: 131792-12-6
3-(1H-Indol-3-yl)-2-(triphenyl-λ⁵-phosphanylidene)-propionic acid benzyl ester

: 134676-38-3
Benzyl (4RS)-(E)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate

Guidance literature:: With sodium periodate; N-methyl-2-indolinone; osmium(VIII) oxide; Yield given. Multistep reaction;
DOI:10.1016/S0040-4039(00)95477-7

Reference yield:

: 134676-37-2
Acetic acid 1-(tert-butoxycarbonylamino-methyl)-allyl ester

: 131792-12-6
3-(1H-Indol-3-yl)-2-(triphenyl-λ⁵-phosphanylidene)-propionic acid benzyl ester

: 134676-38-3
Benzyl (4RS)-(E)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate

: 131792-14-8
Benzyl (4RS)-(Z)-4-Acetoxy-5-<(tert-butoxycarbonyl)amino>-2-(3-indolylmethyl)-2-pentenoate

Guidance literature:: With sodium periodate; N-methyl-2-indolinone; Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1021/jo00006a027